Silane, [(2,3-dimethyl-1-cyclohexen-1-yl)oxy]trimethyl-

Base Information

Chemical Name:Silane, [(2,3-dimethyl-1-cyclohexen-1-yl)oxy]trimethyl-
CAS No.:98361-28-5
Molecular Formula:C11H22OSi
Molecular Weight:198.381
Hs Code.:
DSSTox Substance ID:DTXSID50435287

Synonyms:Silane, [(2,3-dimethyl-1-cyclohexen-1-yl)oxy]trimethyl-;98361-28-5;DTXSID50435287

Suppliers and Price of Silane, [(2,3-dimethyl-1-cyclohexen-1-yl)oxy]trimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Silane, [(2,3-dimethyl-1-cyclohexen-1-yl)oxy]trimethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:198.143991855
Heavy Atom Count:13
Complexity:213

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCCC(=C1C)O[Si](C)(C)C

Technology Process of Silane, [(2,3-dimethyl-1-cyclohexen-1-yl)oxy]trimethyl-

There total 5 articles about Silane, [(2,3-dimethyl-1-cyclohexen-1-yl)oxy]trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 1121-18-2
2-methyl-2-cyclohexen-1-one

: 75-16-1
methylmagnesium bromide

: 98361-28-5
2,3-dimethyl-1-trimethylsilyloxycyclohexene

Guidance literature:: methylmagnesium bromide; With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -40 ℃; for 0.5h; Inert atmosphere;

chloro-trimethyl-silane; 2-methyl-2-cyclohexen-1-one; In tetrahydrofuran; at -40 ℃; for 1h; Inert atmosphere;

With triethylamine; In tetrahydrofuran; Inert atmosphere;
DOI:10.1039/c0cc04725b

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 13395-76-1
2,3-dimethylcyclohexanone

: 98361-28-5
2,3-dimethyl-1-trimethylsilyloxycyclohexene

Guidance literature:: With 1,1,1,3,3,3-hexamethyl-disilazane; sodium iodide; In acetonitrile;
DOI:10.1016/S0040-4039(98)00769-2

Reference yield:

: 1502-24-5
2,3-dimethylcyclohexan-1-ol

: 98361-28-5
2,3-dimethyl-1-trimethylsilyloxycyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridinium chlorochromate (PCC) / CH₂Cl₂ / 2.5 h / Ambient temperature

2: 1) LDA / 1) THF, hexane, -70 deg C, 1.5 h, 2) up to r.t.

With pyridinium chlorochromate; lithium diisopropyl amide; In dichloromethane;