4-Methoxybenzaldehyde N-MethyliMine

Base Information

• Chemical Name: 4-Methoxybenzaldehyde N-MethyliMine
• CAS No.: 13114-23-3
• Molecular Formula: C9H11 N O
• Molecular Weight: 149.192
• Mol file: 13114-23-3.mol

Synonyms:Methylamine,N-(p-methoxybenzylidene)- (6CI,7CI,8CI); 4-Methoxybenzaldehyde N-methylimine;N-(4-Methoxybenzylidene)methylamine; N-(p-Methoxybenzylidene)methylamine;N-Methyl-p-methoxybenzalimine; N-[(4-Methoxyphenyl)methylene]methanamine; NSC146468; [(4-Methoxyphenyl)methylene]methylamine

Chemical Property of 4-Methoxybenzaldehyde N-MethyliMine

Chemical Property:

• Vapor Pressure: 0.0866mmHg at 25°C
• Boiling Point: 233.1°Cat760mmHg
• Flash Point: 79.9°C
• PSA: 21.59000
• Density: 0.94g/cm³
• LogP: 1.74390
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

N-(4-Methoxybenzylidene)methanamine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methoxybenzaldehyde N-MethyliMine

There total 13 articles about 4-Methoxybenzaldehyde N-MethyliMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-methoxy-benzaldehyde (123-11-5) + methylamine (74-89-5) → 4-methoxybenzyl-N-methylimine (13114-23-3)

Guidance literature:

In ethanol; water; at 40 ℃; for 2h;

Reference yield: 100.0%

4-methoxy-benzaldehyde (123-11-5) + methylamine (74-89-5) → N-p-methoxybenzylidenemethylamine (13114-23-3,60682-83-9)

Guidance literature:

With magnesium sulfate; In dichloromethane; for 2h; Reflux;

DOI:10.1021/acs.joc.5b00312

Reference yield: 80.0%

methylamine hydrochloride (593-51-1) + 4-methoxy-benzaldehyde (123-11-5) → 4-methoxybenzyl-N-methylimine (13114-23-3)

Guidance literature:

With 1,1'-(1,4-butanediyl)bis(imidazole); In neat (no solvent); at 20 ℃; for 10h; Milling;

DOI:10.1071/CH18408

upstream raw materials:

methylamine hydrochloride

4-methoxy-benzaldehyde

methylamine

N-Chlor-p-methoxy-benzylmethylamin

Downstream raw materials:

2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-N-methyl-2-phenyl-acetamide

1-methylthio-3-(p-methoxyphenyl)-1,2-cyclopropanedicarboxylic acid diethyl ester

dimethyl amine

3-tert-Butyl-2-(4-methoxyphenyl)-1-methyl-4-thioxo-3-azetidincarbonitril