3,4-Dimethoxythioanisole

Base Information

Chemical Name:3,4-Dimethoxythioanisole
CAS No.:2570-42-5
Molecular Formula:C9H12 O2 S
Molecular Weight:184.259
Hs Code.:2930909090
European Community (EC) Number:673-600-9
DSSTox Substance ID:DTXSID00948574
Nikkaji Number:J1.809.806G
Wikidata:Q82926400
Mol file:2570-42-5.mol

Synonyms:3,4-Dimethoxythioanisole;2570-43-6;1,2-dimethoxy-4-methylsulfanylbenzene;1,2-dimethoxy-4-(methylsulfanyl)benzene;(3,4-dimethoxyphenyl)(methyl)sulfane;3,4-Dimethoxythioanisol;SCHEMBL3511079;DTXSID00948574;1-(Methylthio)-3,4-dimethoxybenzene;AKOS006278641;E97742

Suppliers and Price of 3,4-Dimethoxythioanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(2,5-Dimethoxyphenyl)(methyl)sulfane 97%
5g
$ 1312.00

Total 4 raw suppliers

Chemical Property of 3,4-Dimethoxythioanisole

Chemical Property:

Vapor Pressure:0.0159mmHg at 25°C
Boiling Point:264.4°Cat760mmHg
Flash Point:113.7°C
PSA：43.76000
Density:1.11g/cm³
LogP:2.42570
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:184.05580079
Heavy Atom Count:12
Complexity:130

Purity/Quality:

99% ^*data from raw suppliers

(2,5-Dimethoxyphenyl)(methyl)sulfane 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)SC)OC

Technology Process of 3,4-Dimethoxythioanisole

There total 7 articles about 3,4-Dimethoxythioanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1483-27-8
2,5-dimethoxythiophenol

: 77-78-1
dimethyl sulfate

: 2570-42-5
2-(methylthio)-1,4-dimethoxybenzene

Guidance literature:: 2,5-dimethoxythiophenol; With potassium hydroxide; In methanol; for 1h;

dimethyl sulfate; In methanol; for 0.5h; Heating;
DOI:10.1021/jm0493109

Reference yield: 72.0%

: 624-92-0
Dimethyldisulphide

: 25245-35-6
1-iodo-2,4-dimethoxybenzene

: 2570-42-5
2-(methylthio)-1,4-dimethoxybenzene

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; fac-tris(2-phenylpyridinato-N,C₂')iridium(III); dimethyl sulfoxide; In acetonitrile; at 20 ℃; for 24h; chemoselective reaction; Irradiation; Sealed tube;
DOI:10.1039/c8ob00238j

Reference yield:

: 150-78-7
1,4-dimethoxybezene

: 2570-42-5
2-(methylthio)-1,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 68.3 percent / aq. HOSO₂Cl

2.1: 99 percent / Zn; aq. HCl

3.1: KOH / methanol / 1 h

3.2: 99 percent / methanol / 0.5 h / Heating

With hydrogenchloride; chlorosulfonic acid; potassium hydroxide; zinc; In methanol;
DOI:10.1021/jm0493109