methanediyl bis(4-methoxybenzoate)

Base Information

• Chemical Name: methanediyl bis(4-methoxybenzoate)
• CAS No.: 56741-12-9
• Molecular Formula: C17H16O6
• Molecular Weight: 316.31
• Mol file: 56741-12-9.mol

Synonyms:

Chemical Property of methanediyl bis(4-methoxybenzoate)

Chemical Property:

• Vapor Pressure: 2.21E-09mmHg at 25°C
• Boiling Point: 480.2°Cat760mmHg
• Flash Point: 213.1°C
• Density: 1.227g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methanediyl bis(4-methoxybenzoate)

There total 4 articles about methanediyl bis(4-methoxybenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

dichloromethane (75-09-2) + 4-methoxybenzoic acid (100-09-4) → C17H16O6 (56741-12-9)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In neat (no solvent); at 80 ℃; for 0.75h; Microwave irradiation;

DOI:10.1016/j.cclet.2014.11.001

Reference yield: 90.0%

potassium 4-methoxybenzoate (52509-81-6) + 1,1-dibromomethane (74-95-3) → C17H16O6 (56741-12-9)

Guidance literature:

With poly(ethylene glycol)-600; In acetonitrile; for 13h; Ambient temperature;

DOI:10.1080/00397919708004081

Reference yield: 33.0%

4-methoxybenzoic acid (100-09-4) + 1,1-dibromomethane (74-95-3) → 5-methoxyisobenzofuran-1(3H)-one (4741-62-2) + C17H16O6 (56741-12-9)

Guidance literature:

With palladium diacetate; potassium hydrogencarbonate; at 140 ℃; for 18h; Sealed tube;

DOI:10.1016/j.molstruc.2013.12.059

upstream raw materials:

dichloromethane

4-methoxybenzoic acid

potassium 4-methoxybenzoate

1,1-dibromomethane