Propane, 1,1'-((1E)-1,2-ethenediylbis(thio))bis-

Base Information

• Chemical Name: Propane, 1,1'-((1E)-1,2-ethenediylbis(thio))bis-
• CAS No.: 1120-17-8
• Molecular Formula: C8H16 S2
• Molecular Weight: 176.347
• Hs Code.: 2930909090
• European Community (EC) Number: 214-299-2
• DSSTox Substance ID: DTXSID401244560
• Nikkaji Number: J203.346A
• Mol file: 1120-17-8.mol

Synonyms:1120-17-8;1-[(E)-2-propylsulfanylethenyl]sulfanylpropane;Propane, 1,1'-((1E)-1,2-ethenediylbis(thio))bis-;EINECS 214-299-2;trans-1,2-Bis(n-propylmercapto)ethene;(E)-1,1'-[vinylenebis(thio)]bispropane;(E)-1,1'-(Vinylenebis(thio))bispropane;Propane, 1,1'-[(1E)-1,2-ethenediylbis(thio)]bis-;Propane, 1,1'-(1,2-ethenediylbis(thio))bis-, (E)-;Propane, 1,1'-[1,2-ethenediylbis(thio)]bis-, (E)-;C8H16S2;SCHEMBL8022546;DTXSID401244560;1,1'-[(E)-1,2-Ethenediylbis(thio)]bispropane;1,1'-[(1E)-1,2-Ethenediylbis(thio)]bis[propane]

Chemical Property of Propane, 1,1'-((1E)-1,2-ethenediylbis(thio))bis-

Chemical Property:

• Boiling Point: 247.4oC at 760 mmHg
• Flash Point: 96.6oC
• PSA: 50.60000
• Density: 0.968g/cm3
• LogP: 3.74400
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 176.06934286
• Heavy Atom Count: 10
• Complexity: 69.3

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCSC=CSCCC
• Isomeric SMILES: CCCS/C=C/SCCC

Technology Process of Propane, 1,1'-((1E)-1,2-ethenediylbis(thio))bis-

There total 35 articles about Propane, 1,1'-((1E)-1,2-ethenediylbis(thio))bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

undecyl cyanide (2437-25-4) → lauric acid amide (1120-16-7)

Guidance literature:

With dihydrogen peroxide; hexadecyltrimethylammonium methanesulfonate; sodium hydroxide; In water; at 25 ℃; for 1h;

DOI:10.2174/157017809787582708

Reference yield: 92.0%

Lauroyl azide (43009-32-1) → lauric acid amide (1120-16-7)

Guidance literature:

With zinc(II) tetrahydroborate; In 1,2-dimethoxyethane; for 0.5h; Ambient temperature;

DOI:10.1021/jo00094a021

Reference yield: 89.0%

Dodecanal (112-54-9) → lauric acid (143-07-7) + lauric acid amide (1120-16-7) + undecyl cyanide (2437-25-4)

Guidance literature:

With H₂SO₄*2NH₂OH; Rh(OH)x/Al₂O₃; In water; for 9h; Heating;

DOI:10.1002/anie.200701273

upstream raw materials:

lauric acid

n-dodecanoyl chloride

ethyl laurate

urea

Refernces

• 1、 Coeck, Robin,De Vos, Dirk E.. "One-pot reductive amination of carboxylic acids: a sustainable method for primary amine synthesis". supporting information. p. 5105 - 5114. Retrieved 2020/08/25.
• 2、 Jamil, Md. A. R.,Siddiki, S. M. A. Hakim,Touchy, Abeda Sultana,Rashed, Md. Nurnobi,Poly, Sharmin Sultana,Jing, Yuan,Ting, Kah Wei,Toyao, Takashi,Maeno, Zen,Shimizu, Ken-ichi. "Selective Transformations of Triglycerides into Fatty Amines, Amides, and Nitriles by using Heterogeneous Catalysis". . p. 3115 - 3125. Retrieved 2019/04/26.