Technology Process of N~2~,N~2~,N~4~,N~4~,N~6~,N~6~-Hexakis(trimethylsilyl)-1,3,5,2,4,6-triazatriborinane-2,4,6-triamine
There total 1 articles about N~2~,N~2~,N~4~,N~4~,N~6~,N~6~-Hexakis(trimethylsilyl)-1,3,5,2,4,6-triazatriborinane-2,4,6-triamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
benzene;
Addn. of mixt. of org. materials to a stirred soln. of B-compd. (C6H6) at room temp., stirring (room temp., 115 h).; Filtn. gives 96% of NEt3*HCl and 90% of borazine (obtained from filtrate). Purifn. by crystn. from hexane results in 71% pure material. Elem. anal.;
- Guidance literature:
-
With
hydrogenchloride;
In
benzene;
byproducts: NH4Cl; React. of starting materials (vac., room temp., benzene, 17 h).; Recovery of starting borazine (36.1%), sepn. of volatile materials by fractional condensation (NH4Cl as by product). Identification by combination of use of calibrated traps, quantitative IR anal. and GC/MS.;
- Guidance literature:
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React. of starting materials (vac., 135-150°C, 46 h).; Sepn. of volatile materials by fractional condensation. Identification by combination of use of calibrated traps, quantitative IR anal. and GC/MS.;