Benzeneselenenic acid, 2,4,6-tris(1,1-dimethylethyl)-, methyl ester

Base Information

• Chemical Name: Benzeneselenenic acid, 2,4,6-tris(1,1-dimethylethyl)-, methyl ester
• CAS No.: 114031-54-8
• Molecular Formula: C19H32OSe
• Molecular Weight: 355.422
• Mol file: 114031-54-8.mol

Synonyms:

Chemical Property of Benzeneselenenic acid, 2,4,6-tris(1,1-dimethylethyl)-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of Benzeneselenenic acid, 2,4,6-tris(1,1-dimethylethyl)-, methyl ester

There total 4 articles about Benzeneselenenic acid, 2,4,6-tris(1,1-dimethylethyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

methanol (67-56-1) + bis(2,4,6-tri-tert-butyl)phenyl diselenide (20875-32-5) + 2,4,6-tri-tert-butylbenzeneseleninic acid (114031-56-0) → 2,4,6-tri-tert-Butylbenzeneselenenate (114031-54-8)

Guidance literature:

DOI:10.1021/jo00245a056

Reference yield:

methanol (67-56-1) + N,N-Dimethyl-2,4,6-tri-tert-butylbenzeneselenenamide → 2,4,6-tri-tert-Butylbenzeneselenenate (114031-54-8) + dimethyl amine (124-40-3)

Guidance literature:

With trifluorormethanesulfonic acid; lithium trifluoromethanesulfonate; In acetonitrile; at 25 ℃; Rate constant; Mechanism; influence of concentration of CF₃SO₃H and MeOH;

DOI:10.1021/jo00056a026

Reference yield:

sodium methylate (124-41-4) + 2,4,6-Tri-tert-butylbenzeneselenenyl bromide (114031-59-3) → 2,4,6-tri-tert-Butylbenzeneselenenate (114031-54-8)

Guidance literature:

In methanol;

DOI:10.1021/jo00245a056

upstream raw materials:

methanol

bis(2,4,6-tri-tert-butyl)phenyl diselenide

2,4,6-tri-tert-butylbenzeneseleninic acid

C₁₈H₃₀OSe

Downstream raw materials:

N-Benzyl-Se-(2,4,6-tri-tert-butyl-phenyl)-selenohydroxylamine

C₂₅H₃₆SSe

C₁₉H₃₂O₂Se

C₁₈H₃₀OSe

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