3-(2,5,5-Trimethyl-1,3-dioxan-2-yl)thiophene

Base Information

Chemical Name:3-(2,5,5-Trimethyl-1,3-dioxan-2-yl)thiophene
CAS No.:138890-86-5
Molecular Formula:C11H16O2S
Molecular Weight:212.30900
Hs Code.:
Mol file:138890-86-5.mol

Synonyms:3-(2,5,5-trimethyl-1,3-dioxan-2-yl)thiophene;3-(2,5,5-Trimethyl-1,3-dioxane-2-yl)thiophene;3-(2,5,5-Trimethyl-l,3-dioxane-2-yl)thiophene;

Suppliers and Price of 3-(2,5,5-Trimethyl-1,3-dioxan-2-yl)thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-(2,5,5-Trimethyl-1,3-dioxan-2-yl)thiophene

Chemical Property:

Melting Point:35-37℃
Boiling Point:279℃
Flash Point:122℃
PSA：46.70000
Density:1.066
LogP:2.99380

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(2,5,5-Trimethyl-1,3-dioxan-2-yl)thiophene

There total 2 articles about 3-(2,5,5-Trimethyl-1,3-dioxan-2-yl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1468-83-3
1-(thiophen-3-yl)-ethanone

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 138890-86-5
3-(2,5,5-Trimethyl-l,3-dioxane-2-yl)thiophene

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 24h; Heating / reflux;

Reference yield:

: 1468-83-3
1-(thiophen-3-yl)-ethanone

: 144-55-8
sodium hydrogencarbonate

: 7440-44-0
pyrographite

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 138890-86-5
3-(2,5,5-Trimethyl-l,3-dioxane-2-yl)thiophene

Guidance literature:: With sulfuric acid; potassium carbonate; In hexane; toluene;

Reference yield: 80.0%

: 138890-86-5
3-(2,5,5-Trimethyl-l,3-dioxane-2-yl)thiophene

: 138890-87-6
3-(2,5,5-Trimethyl-1,3-dioxane-2-yl)-thiophene-2-sulfonamide

Guidance literature:: 3-(2,5,5-Trimethyl-l,3-dioxane-2-yl)thiophene; With n-butyllithium; In hexane; at -60 - 20 ℃; for 3.25h; Inert atmosphere;

With sulfur dioxide; In tetrahydrofuran; hexane; at -65 - 20 ℃; Inert atmosphere;

With sodium acetate trihydrate; hydroxylamine-O-sulfonic acid; In water; at 0 - 20 ℃;