2-(Trimethylsiloxy)-1,2,3-propanetricarboxylic acid tris(trimethylsilyl) ester

Base Information

• Chemical Name: 2-(Trimethylsiloxy)-1,2,3-propanetricarboxylic acid tris(trimethylsilyl) ester
• CAS No.: 14330-97-3
• Molecular Formula: C18H40O7Si4
• Molecular Weight: 480.84800
• Mol file: 14330-97-3.mol

Synonyms:tetra-Trimethylsilyl-citronensaeure;Trimethylsilyl-citronensaeure;

Chemical Property of 2-(Trimethylsiloxy)-1,2,3-propanetricarboxylic acid tris(trimethylsilyl) ester

Chemical Property:

• PSA: 88.13000
• LogP: 4.49120

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(Trimethylsiloxy)-1,2,3-propanetricarboxylic acid tris(trimethylsilyl) ester

There total 3 articles about 2-(Trimethylsiloxy)-1,2,3-propanetricarboxylic acid tris(trimethylsilyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) + citric acid (77-92-9,906507-37-7) → citric acid tetrakistrimethylsilane (14330-97-3)

Guidance literature:

With chloro-trimethyl-silane; at 70 ℃; for 4h;

DOI:10.1021/jf030751v

Reference yield:

chloro-trimethyl-silane (75-77-4) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) + citric acid (77-92-9,906507-37-7) → citric acid tetrakistrimethylsilane (14330-97-3)

Guidance literature:

With pyridine;

DOI:10.1139/v72-616

Reference yield:

→ citric acid tetrakistrimethylsilane (14330-97-3)

Guidance literature:

Spinnegift, N,O-Bis-(trimethylsilyl)-trifluoracetamid (EIMS);

DOI:10.1002/bms.1200060305

upstream raw materials:

chloro-trimethyl-silane

1,1,1,3,3,3-hexamethyl-disilazane

citric acid

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