Propane, 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoro-

Base Information

• Chemical Name: Propane, 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoro-
• CAS No.: 677-68-9
• Molecular Formula: C3Cl4 F4
• Molecular Weight: 253.839
• DSSTox Substance ID: DTXSID30865482
• Nikkaji Number: J50.925F
• Mol file: 677-68-9.mol

Synonyms:Propane, 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoro-;CFC 214;Tetrachlorotetrafluoropropane;677-68-9;1,2,2,3-tetrachloro-1,1,3,3-tetrafluoropropane;1,2,2,3-Tetrachlorotetraflouropropane;BRN 1759305;1,2,2,3-TETRACHLORO-1,1,3,3-TETRAFLUORO-PROPANE;29255-31-0;Propane, tetrachlorotetrafluoro-;4-01-00-00203 (Beilstein Handbook Reference);1,2,2,3-Tetrachloro-1,1,3,3-tetrafluoro propane;C3-Cl4-F4;CFC-214aa;C3Cl4F4;SCHEMBL1222666;DTXSID30865482;1,2,2,3-Tetrachlorotetrafluoropropane;LS-120978;LS-120979

Chemical Property of Propane, 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoro-

Chemical Property:

• Vapor Pressure: 25.9mmHg at 25°C
• Melting Point: -42.9°C
• Refractive Index: 1.3958
• Boiling Point: 112.2°C at 760 mmHg
• Flash Point: 30.1°C
• PSA: 0.00000
• Density: 1.744g/cm³
• LogP: 3.82350
• XLogP3: 4.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 253.866073
• Heavy Atom Count: 11
• Complexity: 139

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(F)(F)Cl)(C(F)(F)Cl)(Cl)Cl

Technology Process of Propane, 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoro-

There total 4 articles about Propane, 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

freon-214 (2268-46-4) → tetrachloromethane (56-23-5) + 1,1,2,2-tetrachloroethylene (127-18-4) + 1,1,1,2-tetrachloro-2,3,3,3-tetrafluoropropane (3175-64-2) + 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoropropane (677-68-9)

Guidance literature:

aluminum (III) chloride; at 115 ℃; for 48h; Inert atmosphere of nitrogen;

Reference yield:

polytetrafluoroethylene (116-14-3,82785-14-6) + Dichlorodifluoromethane (75-71-8) → tetrachloromethane (56-23-5) + 1,3-dichlorohexafluoropropane (662-01-1) + trichlorofluoromethane (75-69-4) + 1,1-dichlorohexafluoropropane (2729-28-4) + 1,1,1-trichloro-2,2,3,3,3-pentafluoropropane (4259-43-2) + 1,1,3-trichloro-1,2,2,3,3-pentafluoropropane (1652-81-9,79070-11-4) + 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoropropane (677-68-9) + 3,3-dichloro-1,1,1,2,2,4,4,5,5,5-decafluoropentane (146721-82-6)

Guidance literature:

AlClxF₃-x; at 60 - 80 ℃; for 2.55h; under 4897.34 - 6759.13 Torr; Product distribution / selectivity; Sealed tube;

Reference yield:

1,1-dichlorotetrafluorocyclopropane (695-49-8) → freon-214 (2268-46-4) + 1,2,2,3-tetrachloro-1,1,3,3-tetrafluoropropane (677-68-9)

Guidance literature:

With chlorine; at 260 ℃; for 10h; Title compound not separated from byproducts;

DOI:10.1021/jo030014y

upstream raw materials:

1,1-dichlorotetrafluorocyclopropane

propane

polytetrafluoroethylene

Dichlorodifluoromethane

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