2-Cyclohexen-1-one, 4-(3,5-dimethoxyphenyl)-3-ethenyl-4-methyl-

Base Information

Chemical Name:2-Cyclohexen-1-one, 4-(3,5-dimethoxyphenyl)-3-ethenyl-4-methyl-
CAS No.:170753-26-1
Molecular Formula:C₁₇H₂₀O₃
Molecular Weight:272.344
Hs Code.:
Mol file:170753-26-1.mol

Synonyms:

Suppliers and Price of 2-Cyclohexen-1-one, 4-(3,5-dimethoxyphenyl)-3-ethenyl-4-methyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclohexen-1-one, 4-(3,5-dimethoxyphenyl)-3-ethenyl-4-methyl-

Chemical Property:

Purity/Quality:

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Technology Process of 2-Cyclohexen-1-one, 4-(3,5-dimethoxyphenyl)-3-ethenyl-4-methyl-

There total 6 articles about 2-Cyclohexen-1-one, 4-(3,5-dimethoxyphenyl)-3-ethenyl-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18917-77-6
(3,5-dimethoxyphenyl)acetone

: 170753-26-1
4-(3',5'-dimethoxyphenyl)-4-methyl-3-vinylcyclohex-2-enone

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / NaH / tetrahydrofuran / 1.) 0 deg C to room temperature, 30 min, 2.) 0 deg C, 1 h; room temperature, 4 h

2: 151 mg / t-BuOK / tetrahydrofuran / 1.) 30 min, 2.) 3 d

3: 83 percent / p-TsOH / 2 h / Heating

4: 1.) cerium chloride, 2.) 2percent HCl / 1.) THF, room temperature, 4 h, 2.) 20 min

With hydrogenchloride; cerium(III) chloride; potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran;
DOI:10.1021/jo970570q

Reference yield:

: 15601-07-7
2-(3,5-dimethoxyphenyl)acetyl chloride

: 170753-26-1
4-(3',5'-dimethoxyphenyl)-4-methyl-3-vinylcyclohex-2-enone

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / diethyl ether / 1 h / -78 °C

2: 97 percent / NaH / tetrahydrofuran / 1.) 0 deg C to room temperature, 30 min, 2.) 0 deg C, 1 h; room temperature, 4 h

3: 151 mg / t-BuOK / tetrahydrofuran / 1.) 30 min, 2.) 3 d

4: 83 percent / p-TsOH / 2 h / Heating

5: 1.) cerium chloride, 2.) 2percent HCl / 1.) THF, room temperature, 4 h, 2.) 20 min

With hydrogenchloride; cerium(III) chloride; potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo970570q

Reference yield:

: 4670-10-4
(3,5-dimethoxyphenyl)acetic acid

: 170753-26-1
4-(3',5'-dimethoxyphenyl)-4-methyl-3-vinylcyclohex-2-enone

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / oxalyl chloride / benzene / 17 h / Ambient temperature

2: 64 percent / diethyl ether / 1 h / -78 °C

3: 97 percent / NaH / tetrahydrofuran / 1.) 0 deg C to room temperature, 30 min, 2.) 0 deg C, 1 h; room temperature, 4 h

4: 151 mg / t-BuOK / tetrahydrofuran / 1.) 30 min, 2.) 3 d

5: 83 percent / p-TsOH / 2 h / Heating

6: 1.) cerium chloride, 2.) 2percent HCl / 1.) THF, room temperature, 4 h, 2.) 20 min

With hydrogenchloride; cerium(III) chloride; oxalyl dichloride; potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo970570q