N-(3-Acetylphenyl)-N-ethylacetaMide

Base Information

Chemical Name:N-(3-Acetylphenyl)-N-ethylacetaMide
CAS No.:200630-96-2
Molecular Formula:C12H15NO2
Molecular Weight:205.257
Hs Code.:
Mol file:200630-96-2.mol

Synonyms:N-(3-acetyl-phenyl)-N-ethyl-acetamide;N-(3-acetylphenyl)-N-ethylacetamide;

Suppliers and Price of N-(3-Acetylphenyl)-N-ethylacetaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-(3-Acetylphenyl)-N-ethylacetamide
2.5g
$ 1320.00

Medical Isotopes, Inc.
N-(3-Acetylphenyl)-N-ethylacetamide
250 mg
$ 650.00

Total 1 raw suppliers

Chemical Property of N-(3-Acetylphenyl)-N-ethylacetaMide

Chemical Property:

PSA：37.38000
LogP:2.26200
Storage Temp.:-20°C Freezer, Under inert atmosphere
Solubility.:Chloroform, Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:: N-(3-Acetylphenyl)-N-ethylacetamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses N-(3-Acetylphenyl)-N-ethylacetamide is a reactant used in the preparation of 5-Oxo-Zaleplon (O870470), a metabolite of Zaleplon (Z145000).

Technology Process of N-(3-Acetylphenyl)-N-ethylacetaMide

There total 5 articles about N-(3-Acetylphenyl)-N-ethylacetaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 7463-31-2
3-Acetamidoacetophenone

: 75-03-6
ethyl iodide

: 200630-96-2
N-(3-acetylphenyl)-N-ethylacetamide

Guidance literature:: With potassium hydroxide; In acetone; at 20 ℃;

Reference yield: 75.0%

: 557-20-0
diethylzinc

: 75-36-5
acetyl chloride

: 121-89-1
3-Nitroacetophenone

: 200630-96-2
N-(3-acetylphenyl)-N-ethylacetamide

Guidance literature:: diethylzinc; 3-Nitroacetophenone; With triethylamine; bis(pinacol)diborane; In hexane; toluene; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere;

acetyl chloride; In hexane; toluene; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201705356

Reference yield:

: 74-96-4
ethyl bromide

: 7463-31-2
3-Acetamidoacetophenone

: 200630-96-2
N-(3-acetylphenyl)-N-ethylacetamide

Guidance literature:: 3-Acetamidoacetophenone; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 40 ℃; for 1h;

ethyl bromide; In N,N-dimethyl-formamide; mineral oil; at 5 - 10 ℃; for 5h;