1-(6-Chloropyridin-3-yl)ethanol

Base Information

Chemical Name:1-(6-Chloropyridin-3-yl)ethanol
CAS No.:23092-75-3
Molecular Formula:C7H8ClNO
Molecular Weight:157.59800
Hs Code.:
Mol file:23092-75-3.mol

Synonyms:1-(6-Chloro-pyridin-3-yl)-ethanol;2-chloro-5-(1-hydroxyethyl)pyridine;1-(6-chloropyridyl)ethanol;2-Chlor-5-(α-hydroxy-ethyl)-pyridin;-(6-chloropyridin-3-yl)ethanol;

Suppliers and Price of 1-(6-Chloropyridin-3-yl)ethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(6-Chloropyridin-3-yl)ethanol 97%
1g
$ 552.00

Acrotein
6-Chloro-a-methyl-3-pyridinemethanol 97%
0.5g
$ 220.00

AccelPharmtech
6-chloro-a-methyl-3-Pyridinemethanol 97.00%
25G
$ 5120.00

AccelPharmtech
6-chloro-a-methyl-3-Pyridinemethanol 97.00%
5G
$ 2750.00

AccelPharmtech
6-chloro-a-methyl-3-Pyridinemethanol 97.00%
1G
$ 2370.00

Total 6 raw suppliers

Chemical Property of 1-(6-Chloropyridin-3-yl)ethanol

Chemical Property:

Boiling Point:109 - 110 °C (0.05 mmHg)
PKA:13.39±0.20(Predicted)
PSA：33.12000
Density:1.253±0.06 g/cm3(Predicted)
LogP:1.78830

Purity/Quality:

99% ^*data from raw suppliers

1-(6-Chloropyridin-3-yl)ethanol 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(6-Chloropyridin-3-yl)ethanol

There total 6 articles about 1-(6-Chloropyridin-3-yl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.2%

: 55676-22-7
3-acetyl-6-chloropyridine

: 23092-75-3
1-(6-chloropyridin-3-yl)ethanol

Guidance literature:: With sodium tetrahydroborate; In ethanol; water; at 20 ℃;
DOI:10.1271/bbb.67.980

Reference yield:

: 23100-12-1
6-chloronicotinylaldehyde

: 676-58-4
methylmagnesium chloride

: 23092-75-3
1-(6-chloropyridin-3-yl)ethanol

Guidance literature:: In tetrahydrofuran; for 0.5h; Inert atmosphere; Cooling with ice;

Reference yield:

: 58757-38-3
6-Chloronicotinoyl chloride

: 23092-75-3
1-(6-chloropyridin-3-yl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 64.7 percent / Fe(CH₂COCH₂COMe)3 / tetrahydrofuran / 3 h / -30 °C

2: 69.2 percent / NaBH₄ / ethanol; H₂O / 20 °C

With sodium tetrahydroborate; Fe(CH₂COCH₂COMe)3; In tetrahydrofuran; ethanol; water;
DOI:10.1271/bbb.67.980