ethyl 3-cyano-5-Methylhex-3-enoate

Base Information

Chemical Name:ethyl 3-cyano-5-Methylhex-3-enoate
CAS No.:350801-68-2
Molecular Formula:C10H15NO2
Molecular Weight:181.235
Hs Code.:
Mol file:350801-68-2.mol

Synonyms:(E)-3-Cyano-5-methyl-hex-3-enoic acid ethyl ester;ethyl 3-cyano-5-methyl hex-3-enoate;

Suppliers and Price of ethyl 3-cyano-5-Methylhex-3-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of ethyl 3-cyano-5-Methylhex-3-enoate

Chemical Property:

Vapor Pressure:0.00281mmHg at 25°C
Boiling Point:285℃
Flash Point:130℃
PSA：50.09000
Density:0.983
LogP:2.04558

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of ethyl 3-cyano-5-Methylhex-3-enoate

There total 4 articles about ethyl 3-cyano-5-Methylhex-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 350801-67-1
carbonic acid 2-cyano-1-isopropyl-allyl ester ethyl ester

: 350801-68-2
3-cyano-5-methyl-hex-3-enoic acid ethyl ester

Guidance literature:: With triphenylphosphine; palladium diacetate; at 50 ℃; under 14480.1 - 15514.4 Torr;
DOI:10.1021/jo034397b

Reference yield:

: dimethylphosphono(3-cyano)propionic acid ethyl ester

: 78-84-2
isobutyraldehyde

: 350801-68-2
3-cyano-5-methyl-hex-3-enoic acid ethyl ester

Guidance literature:: dimethylphosphono(3-cyano)propionic acid ethyl ester; With sodium hydride; In tetrahydrofuran; at 0 ℃;

isobutyraldehyde; In tetrahydrofuran; at 0 ℃; for 5h; Temperature; Time;

Reference yield:

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 166327-69-1
acetic acid 2-cyano-1-isopropyl-allyl ester

: 350801-68-2
3-cyano-5-methyl-hex-3-enoic acid ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium bromide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; at 50 ℃; for 24h; under 2068.65 - 2585.81 Torr; Product distribution / selectivity;