1,3-Dioxolane, 2-methyl-2-(2-nitrophenyl)-

Base Information

Chemical Name:1,3-Dioxolane, 2-methyl-2-(2-nitrophenyl)-
CAS No.:37456-50-1
Molecular Formula:C10H11NO4
Molecular Weight:209.202
Hs Code.:
Mol file:37456-50-1.mol

Synonyms:Benzene,1-(2-methyl-1,3-dioxolan-2-yl)-2-nitro;1,3-Dioxolane,2-methyl-2-(2-nitrophenyl);

Suppliers and Price of 1,3-Dioxolane, 2-methyl-2-(2-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1,3-Dioxolane, 2-methyl-2-(2-nitrophenyl)-

Chemical Property:

Melting Point:66 °C
Boiling Point:325.6±37.0 °C(Predicted)
PSA：64.28000
Density:1.265±0.06 g/cm3(Predicted)
LogP:2.33750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Dioxolane, 2-methyl-2-(2-nitrophenyl)-

There total 4 articles about 1,3-Dioxolane, 2-methyl-2-(2-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 577-59-3
2-acetylnitrobenzene

: 107-21-1
ethylene glycol

: 37456-50-1
2-methyl-2-(2-nitrophenyl)-1,3-dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 20h; Heating;
DOI:10.1021/jm00105a017

Reference yield:

: 3674-77-9
2-methyl-2-phenyl-1,3-dioxolane

: 19073-15-5
2-(4-nitrophenyl)-2-methyl-1,3-dioxolane

: 51226-13-2
2-methyl-2-(3-nitrophenyl)-[1,3]dioxolane

: 37456-50-1
2-methyl-2-(2-nitrophenyl)-1,3-dioxolane

: 98-86-2
acetophenone

: 2-benzoyloxyethyl nitrate

Guidance literature:: With oxygen; magnesium oxide; Nitrogen dioxide; ozone; In dichloromethane; at 0 ℃; Product distribution; other acetals;

Reference yield:

: 3674-77-9
2-methyl-2-phenyl-1,3-dioxolane

: 19073-15-5
2-(4-nitrophenyl)-2-methyl-1,3-dioxolane

: 51226-13-2
2-methyl-2-(3-nitrophenyl)-[1,3]dioxolane

: 37456-50-1
2-methyl-2-(2-nitrophenyl)-1,3-dioxolane

Guidance literature:: With magnesium oxide; Nitrogen dioxide; ozone; In acetonitrile; at 0 ℃; for 1.5h; Yield given. Yields of byproduct given;
DOI:10.1246/bcsj.68.1535