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1,3-Propanedione, 1-[1,1'-biphenyl]-4-yl-3-phenyl-

Base Information Edit
  • Chemical Name:1,3-Propanedione, 1-[1,1'-biphenyl]-4-yl-3-phenyl-
  • CAS No.:37974-77-9
  • Molecular Formula:C21H16O2
  • Molecular Weight:300.357
  • Hs Code.:
  • Mol file:37974-77-9.mol
1,3-Propanedione, 1-[1,1'-biphenyl]-4-yl-3-phenyl-

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Chemical Property of 1,3-Propanedione, 1-[1,1'-biphenyl]-4-yl-3-phenyl- Edit
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Technology Process of 1,3-Propanedione, 1-[1,1'-biphenyl]-4-yl-3-phenyl-

There total 7 articles about 1,3-Propanedione, 1-[1,1'-biphenyl]-4-yl-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With aluminum (III) chloride; In dichloromethane; at 0 ℃; for 12h; Inert atmosphere;
Guidance literature:
biphenyl-4-acetaldehyde; In toluene; at 0 ℃; for 0.5h; Inert atmosphere;
With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at 0 ℃; for 0.5h; Inert atmosphere;
benzoyl chloride; In tetrahydrofuran; toluene; for 0.0333333h; Inert atmosphere;
DOI:10.1021/acs.joc.0c02366
Guidance literature:
methyl 2-([1,1'-biphenyl]-4-yl)-2-oxoacetate; α-bromoacetophenone; With potassium carbonate; In 1-methyl-pyrrolidin-2-one; methanol; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere;
With potassium hydroxide; In 1-methyl-pyrrolidin-2-one; methanol; water; at 20 ℃; for 2h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.6b02575
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