Technology Process of Phenol, 2,6-bis(1,1-dimethylethyl)-, propanoate
There total 1 articles about Phenol, 2,6-bis(1,1-dimethylethyl)-, propanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
tetrahydrofuran; hexane;
0 deg C, 30 min and 12 h, 20 deg C;
- Guidance literature:
-
(2,6-di-t-butyl)-phenyl propanoate;
With
tert.-butyl lithium;
In
tetrahydrofuran;
at -78 ℃;
for 0.5h;
Inert atmosphere;
benzaldehyde;
In
tetrahydrofuran;
at -78 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1021/acs.orglett.9b02069
- Guidance literature:
-
(2,6-di-t-butyl)-phenyl propanoate;
With
tert.-butyl lithium;
In
tetrahydrofuran; pentane;
at -78 - 0 ℃;
for 2.5h;
Inert atmosphere;
With
ethylene dibromide;
In
tetrahydrofuran; pentane;
at 0 ℃;
for 0.5h;
Inert atmosphere;
benzophenone;
In
tetrahydrofuran; pentane;
at 0 - 20 ℃;
for 0.166667h;
Reagent/catalyst;
Temperature;
Inert atmosphere;
DOI:10.1021/acs.orglett.9b02069
