3-BroMo-5-cyanobenzoic acid Methyl ester

Base Information

Chemical Name:3-BroMo-5-cyanobenzoic acid Methyl ester
CAS No.:453566-15-9
Molecular Formula:C9H6BrNO2
Molecular Weight:240.056
Hs Code.:2926909090
Mol file:453566-15-9.mol

Synonyms:

Suppliers and Price of 3-BroMo-5-cyanobenzoic acid Methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
3-Bromo-5-cyanobenzoic acid methyl ester
1 g
$ 253.00

SynQuest Laboratories
3-Bromo-5-cyanobenzoic acid methyl ester
250 mg
$ 103.00

SynChem
3-Bromo-5-cyanobenzoic acid methyl ester 95+%
1 g
$ 300.00

Labseeker
3-BroMo-5-cyanobenzoicacidMethylester 95
10g
$ 1716.00

Chemenu
Methyl3-bromo-5-cyanobenzoate 95+%
10g
$ 850.00

American Custom Chemicals Corporation
METHYL-3-BROMO-5-CYANOBENZOATE 95.00%
5MG
$ 497.64

Ambeed
Methyl3-bromo-5-cyanobenzoate 98%
1g
$ 76.00

Ambeed
Methyl3-bromo-5-cyanobenzoate 98%
250mg
$ 27.00

AK Scientific
3-Bromo-5-cyanobenzoicacidmethylester
100mg
$ 95.00

Total 27 raw suppliers

Chemical Property of 3-BroMo-5-cyanobenzoic acid Methyl ester

Chemical Property:

Boiling Point:301.3±27.0 °C(Predicted)
PSA：50.09000
Density:1.60±0.1 g/cm3(Predicted)
LogP:2.10738
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-5-cyanobenzoic acid methyl ester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-BroMo-5-cyanobenzoic acid Methyl ester

There total 7 articles about 3-BroMo-5-cyanobenzoic acid Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1427407-54-2
methyl 3-bromo-5-carbamoyl-benzoate

: 453566-15-9
methyl 3-bromo-5-cyanobenzoate

Guidance literature:: With trichlorophosphate; at 100 ℃;

Reference yield: 50.0%

: 188813-07-2
methyl 3-bromo-5-iodobenzoate

: 453566-15-9
methyl 3-bromo-5-cyanobenzoate

Guidance literature:: With zinc(II) cyanide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

Reference yield:

: 51760-21-5
dimethyl 5-bromoisophthalate

: 453566-15-9
methyl 3-bromo-5-cyanobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C

2: thionyl chloride / Reflux

3: ammonia / tetrahydrofuran

4: trichlorophosphate / 100 °C

With thionyl chloride; lithium hydroxide monohydrate; ammonia; water; trichlorophosphate; In tetrahydrofuran;