5-CHLORO-2-METHYLBENZOIC ACID ETHYL ESTER

Base Information

• Chemical Name: 5-CHLORO-2-METHYLBENZOIC ACID ETHYL ESTER
• CAS No.: 56427-54-4
• Molecular Formula: C10H11ClO2
• Molecular Weight: 198.649
• Hs Code.: 2916399090
• Mol file: 56427-54-4.mol

Synonyms:5-CHLORO-2-METHYLBENZOIC ACID ETHYL ESTER;5-Chlor-2-methyl-benzoesaeure-aethylester;ethyl 5-chloro-o-toluate;QC-7538;

Chemical Property of 5-CHLORO-2-METHYLBENZOIC ACID ETHYL ESTER

Chemical Property:

• Vapor Pressure: 0.0103mmHg at 25°C
• Boiling Point: 263.4oC at 760 mmHg
• Flash Point: 121.9oC
• PSA: 26.30000
• Density: 1.154g/cm3
• LogP: 2.82510
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

Ethyl5-Chloro-2-methylbenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-CHLORO-2-METHYLBENZOIC ACID ETHYL ESTER

There total 2 articles about 5-CHLORO-2-METHYLBENZOIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

5-chloro-2-methylbenzoic acid (7499-06-1) + ethyl iodide (75-03-6) → 5-chloro-2-methyl-benzoic acid ethyl ester (56427-54-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

DOI:10.1002/chem.201502140

Reference yield: 87.0%

ethanol (64-17-5) + 5-chloro-2-methylbenzoic acid (7499-06-1) → 5-chloro-2-methyl-benzoic acid ethyl ester (56427-54-4)

Guidance literature:

With sulfuric acid; for 48h; Heating / reflux;

Reference yield: 68.0%

5-chloro-2-methyl-benzoic acid ethyl ester (56427-54-4) → ethyl α-bromo-5-chloro-o-toluate

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In 1,2-dichloro-ethane; at 75 ℃; for 4h;

upstream raw materials:

ethanol

5-chloro-2-methylbenzoic acid

ethyl iodide

Downstream raw materials:

2-phenoxymethyl-5-chlorobenzoic acid

5-chloro-2-((4-chlorophenoxy)methyl)benzoic acid

5-chloro-2-[(3-chlorophenoxy)methyl]benzoic acid

5-chloro-2-[(2-chlorophenoxy)methyl]benzoic acid

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