2-(4-Nitrophenyl)pyridine

Base Information

• Chemical Name: 2-(4-Nitrophenyl)pyridine
• CAS No.: 4282-47-7
• Molecular Formula: C11H8N2O2
• Molecular Weight: 200.197
• Hs Code.: 2933399090
• Mol file: 4282-47-7.mol

Synonyms:Pyridine,2-(p-nitrophenyl)- (6CI,7CI,8CI);1-Nitro-4-(2-pyridyl)benzene;2-(4-Nitrophenyl)pyridine;2-(p-Nitrophenyl)pyridine;4-(2-Pyridyl)nitrobenzene;

Chemical Property of 2-(4-Nitrophenyl)pyridine

Chemical Property:

• Vapor Pressure: 0.000134mmHg at 25°C
• Melting Point: 116-118 °C
• Refractive Index: 1.611
• Boiling Point: 354.3 °C at 760 mmHg
• PKA: 3.66±0.25(Predicted)
• Flash Point: 168.1 °C
• PSA: 58.71000
• Density: 1.252 g/cm³
• LogP: 3.18000
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-(4-NITROPHENYL)PYRIDINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 2-(4-Nitrophenyl)pyridine

There total 61 articles about 2-(4-Nitrophenyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.8%

4-nitro-benzoyl chloride (122-04-3) + N-butylamine (109-73-9,85404-21-3) → 2-(4-nitrophenyl)pyridine (4282-47-7)

Guidance literature:

With dmap; copper(II) ethylacetoacetate; C₂₆H₃₆NP; silver(I) acetate; In toluene; at 80 ℃; for 10h; Reagent/catalyst;

Reference yield: 94.0%

Trimethylenediamine (109-76-2,54018-94-9) + (4-nitrophenyl)ethanone (100-19-6) → 2-(4-nitrophenyl)pyridine (4282-47-7)

Guidance literature:

With oxygen; palladium diacetate; toluene-4-sulfonic acid; In tetrahydrofuran; for 12h; Reflux;

DOI:10.1016/j.tetlet.2016.12.075

Reference yield: 93.0%

C10H13BNO3(1-)*C16H36N(1+) + 4-chlorobenzonitrile (100-00-5) → 2-(4-nitrophenyl)pyridine (4282-47-7)

Guidance literature:

With (2-hydroxyethyl)(methyl)amine; copper(l) iodide; dichloro(1,3-bis(dicyclohexylphosphino)propane)palladium; In N,N-dimethyl-formamide; at 100 ℃; for 16h; Reagent/catalyst; Inert atmosphere;

DOI:10.1021/ol402268g

upstream raw materials:

pyridine

3,3-dimethyl-1-(4-nitrophenyl)triazene

bis-(4-nitro-phenyldiazenyl)-sulfane

4-nitrobenzenediazonium chloride

Downstream raw materials:

4-(pyridin-2-yl)aniline

2-(p-nitrophenyl)pyridine N-oxide

4-pyridin-2-yl-phenol

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