ethyl 2-methyl-2-(methylamino)propanoate

Base Information

• Chemical Name: ethyl 2-methyl-2-(methylamino)propanoate
• CAS No.: 58743-30-9
• Molecular Formula: C7H15NO2
• Molecular Weight: 145.19900
• Mol file: 58743-30-9.mol

Synonyms:2-methylamino-2-methylpropionitrile;2-cyano-2-methylaminopropane;2-methyl-2-methylamino-propionitrile;2-methylamino-2-methylpropanenitrile;2-Methylamino-2-methylpropionsaeureethylester;2-methylamino-2-cyano-propane;N-Methylaminoisobutyronitril;

Chemical Property of ethyl 2-methyl-2-(methylamino)propanoate

Chemical Property:

• PSA: 38.33000
• LogP: 0.93840

Purity/Quality:

99% ^*data from raw suppliers

ethyl2-methyl-2-(methylamino)propanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 2-methyl-2-(methylamino)propanoate

There total 2 articles about ethyl 2-methyl-2-(methylamino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + 2-methylamino-2-methylpropanenitrile (2273-39-4) → 2-Methyl-2-(methylamino)propionsaeure-ethylester (58743-30-9)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/ja01164a087

Reference yield:

ethanol (64-17-5) + 2-bromo-2-methylpropionic acid (2052-01-9) + methylamine (74-89-5) → 2-Methyl-2-(methylamino)propionsaeure-ethylester (58743-30-9)

Guidance literature:

Multistep reaction; (i) /BRN= 741851/, (ii) /BRN= 1718733/, HCl;

Reference yield: 75.0%

2-Methyl-2-(methylamino)propionsaeure-ethylester (58743-30-9) + benzenesulfonyl chloride (1939-99-7) → 2-<(N-Methyl)-phenylmethansulfonamido>-2-methylpropionsaeureethylester (58742-80-6)

Guidance literature:

With triethylamine; In diethyl ether; at 20 ℃; for 1h;

DOI:10.1002/ardp.19853180405

upstream raw materials:

ethanol

2-methylamino-2-methylpropanenitrile

2-bromo-2-methylpropionic acid

methylamine

Downstream raw materials:

N-Methyl-2-amino-2-methyl-1-propanol

2-<(N-Methyl)-phenylmethansulfonamido>-2-methylpropionsaeureethylester

5-Phenyl-2,3,3-trimethylisothiazolidin-4-on-1,1-dioxid

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