Methyl 3-amino-4-chlorobenzoate

Base Information

• Chemical Name: Methyl 3-amino-4-chlorobenzoate
• CAS No.: 40872-87-5
• Molecular Formula: C8H8ClNO2
• Molecular Weight: 185.61
• Hs Code.: 2922499990
• Mol file: 40872-87-5.mol

Synonyms:2-Chloro-5-methoxycarbonylaniline;3-Amino-4-chlorobenzoic acid methyl ester;Methyl 3-amino-4-chlorobenzoate;

Chemical Property of Methyl 3-amino-4-chlorobenzoate

Chemical Property:

• Vapor Pressure: 0.00188mmHg at 25°C
• Melting Point: 83 °C
• Refractive Index: 1.58
• Boiling Point: 292.1 °C at 760 mmHg
• Flash Point: 130.4 °C
• PSA: 52.32000
• Density: 1.311 g/cm³
• LogP: 2.29000
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

98% ^*data from raw suppliers

Methyl 3-Amino-4-chlorobenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of Methyl 3-amino-4-chlorobenzoate

There total 8 articles about Methyl 3-amino-4-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + 3-amino-4-chloro-benzoic acid (2840-28-0) → methyl 3-amino-4-chlorobenzoate (40872-87-5)

Guidance literature:

With thionyl chloride; at 0 ℃; for 12h; Reflux;

Reference yield: 92.0%

methyl 3-nitro-4-chlorobenzoate (14719-83-6) → methyl 3-amino-4-chlorobenzoate (40872-87-5)

Guidance literature:

With tin(ll) chloride; In methanol; for 1h; Reflux;

DOI:10.1021/jm9016366

Reference yield: 91.0%

methylene chloride (74-87-3) + 3-amino-4-chloro-benzoic acid (2840-28-0) → methyl 3-amino-4-chlorobenzoate (40872-87-5)

Guidance literature:

With thionyl chloride; In methanol; at 0 - 20 ℃;

DOI:10.1021/jm2007084

upstream raw materials:

methyl 3-nitro-4-chlorobenzoate

3-amino-4-chloro-benzoic acid

methanol

2-amino-3-chlorobenzoic acid

Downstream raw materials:

4-Chloro-3-(3-chlorocarbonyl-benzoylamino)-benzoyl chloride

3-amino-4-chloro-2-[2-(2,2-dimethyl-propionyloxy)-1-methylsulfanyl-ethyl]-benzoic acid methyl ester

3-(2-carboxyphenylamino)-4-chlorobenzoic acid methyl ester

7-chloro-1H-indole-4-carboxylic acid methyl ester

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