1-Allyl-3-methylimidazolium iodide

Base Information

• Chemical Name: 1-Allyl-3-methylimidazolium iodide
• CAS No.: 65039-07-8
• Molecular Formula: C7H11N2.I
• Molecular Weight: 250.082
• European Community (EC) Number: 663-160-6
• Mol file: 65039-07-8.mol

Synonyms:1-Allyl-3-methylimidazolium iodide;65039-07-8;3-Allyl-1-methyl-1H-imidazol-3-ium iodide;SCHEMBL380492;MFCD18251336;1-Allyl-3-methylimidazolium iodide, 98%;FT-0696744;1-methyl-3-prop-2-enylimidazol-1-ium;iodide;1-methyl-3-(prop-2-en-1-yl)-1H-imidazol-3-ium iodide

Chemical Property of 1-Allyl-3-methylimidazolium iodide

Chemical Property:

• Melting Point: 65 °C(Solv: toluene (108-88-3))
• PSA: 8.81000
• LogP: -2.49740
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 249.99670
• Heavy Atom Count: 10
• Complexity: 101

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-Allyl-3-methylimidazolium iodide 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 9511928
• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=CN(C=C1)CC=C.[I-]

Technology Process of 1-Allyl-3-methylimidazolium iodide

There total 2 articles about 1-Allyl-3-methylimidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-methyl-1H-imidazole (616-47-7) + allyl iodid (556-56-9) → N-allyl-N'-methylimidazolium iodide (65039-07-8)

Guidance literature:

In acetonitrile; at 50 ℃; for 48h; Sealed tube;

DOI:10.1002/ijch.202100087

Reference yield:

1-allylimidazole (31410-01-2) + methyl iodide (74-88-4) → N-allyl-N'-methylimidazolium iodide (65039-07-8)

Guidance literature:

In dichloromethane; for 1h;

DOI:10.1002/chem.201601343

Reference yield:

bis(trifluoromethane)sulfonimide lithium (90076-65-6) + N-allyl-N'-methylimidazolium iodide (65039-07-8) → 1-allyl-3-methylimidazol-3-ium N-bis(trifluoromethanesulfonyl)imidate (655249-87-9)

Guidance literature:

In water; at 20 ℃; for 24h;

DOI:10.1002/zaac.201600437

upstream raw materials:

1-methyl-1H-imidazole

allyl iodid

1-allylimidazole

methyl iodide

Downstream raw materials:

1-allyl-3-methylimidazol-3-ium N-bis(trifluoromethanesulfonyl)imidate