Hydantoin, 5,5-dimethyl-3-(p-methoxyphenyl)-

Base Information

• Chemical Name: Hydantoin, 5,5-dimethyl-3-(p-methoxyphenyl)-
• CAS No.: 92668-55-8
• Molecular Formula: C12H14N2O3
• Molecular Weight: 234.2512
• DSSTox Substance ID: DTXSID60239091
• Wikidata: Q83121439

Synonyms:BRN 5542373;Hydantoin, 5,5-dimethyl-3-(p-methoxyphenyl)-;3-(p-Methoxyphenyl)-5,5-dimethylhydantoin;2,4-Imidazolidinedione, 3-(4-methoxyphenyl)-5,5-dimethyl-;92668-55-8;DTXSID60239091;LS-76129

Chemical Property of Hydantoin, 5,5-dimethyl-3-(p-methoxyphenyl)-

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.198g/cm³
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 234.10044231
• Heavy Atom Count: 17
• Complexity: 333

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(C(=O)N(C(=O)N1)C2=CC=C(C=C2)OC)C

Technology Process of Hydantoin, 5,5-dimethyl-3-(p-methoxyphenyl)-

There total 10 articles about Hydantoin, 5,5-dimethyl-3-(p-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

5,5-dimethyl-imidazolidine-2,4-dione (77-71-4) + bis(4-anisyl)iodonium triflate (141339-54-0) → 3-(4-methoxyphenyl)-5,5-dimethylimidazolidine-2,4-dione (92668-55-8)

Guidance literature:

With potassium phosphate; copper(l) iodide; In 1,2-dichloro-ethane; at 20 ℃; for 8h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1002/ejoc.202001353

Reference yield: 59.0%

5,5-dimethyl-imidazolidine-2,4-dione (77-71-4) + 4-methoxyphenylboronic acid (5720-07-0) → 3-(4-methoxyphenyl)-5,5-dimethylimidazolidine-2,4-dione (92668-55-8)

Guidance literature:

With pyridine; oxygen; copper diacetate; In dichloromethane; for 168h;

DOI:10.1055/s-2006-949638

Reference yield: 32.0%

5,5-dimethyl-imidazolidine-2,4-dione (77-71-4) + tris(4-methoxyphenyl)bismuth (33397-21-6) → 3-(4-methoxyphenyl)-5,5-dimethylimidazolidine-2,4-dione (92668-55-8)

Guidance literature:

With pyridine; copper diacetate; In dichloromethane; at 20 ℃;

DOI:10.1055/s-2006-949638

upstream raw materials:

5,5-dimethyl-imidazolidine-2,4-dione

4-methoxyphenylboronic acid

tris(4-methoxyphenyl)bismuth

4-methoxy-aniline

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