TRIMETHYLSILYLMETHANETHIOL

Base Information

• Chemical Name: TRIMETHYLSILYLMETHANETHIOL
• CAS No.: 18165-76-9
• Molecular Formula: C4H12 S Si
• Molecular Weight: 120.29
• Hs Code.: 2931900090
• Mol file: 18165-76-9.mol

Synonyms:Methanethiol,(trimethylsilyl)- (6CI,8CI,9CI); (Trimethylsilyl)methanethiol;(Trimethylsilyl)methyl mercaptan; Mercaptomethyltrimethylsilane

Chemical Property of TRIMETHYLSILYLMETHANETHIOL

Chemical Property:

• Refractive Index: 1.4470 to 1.4510
• Boiling Point: 113.1°Cat760mmHg
• PKA: 10.42±0.10(Predicted)
• Flash Point: 22.2°C
• PSA: 38.80000
• Density: 0.833g/cm³
• LogP: 2.21190

Purity/Quality:

98%,99%, ^*data from raw suppliers

Trimethylsilylmethanethiol >97.0%(GC) ^*data from reagent suppliers

Safty Information:

• Statements: 10
• Safety Statements: 16

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TRIMETHYLSILYLMETHANETHIOL

There total 7 articles about TRIMETHYLSILYLMETHANETHIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

thiourea (17356-08-0) + Chloromethyltrimethylsilane (2344-80-1) → trimethylsilanyl-methanethiol (18165-76-9)

Guidance literature:

In ethanol; for 96h; Reflux;

DOI:10.1016/j.ejmech.2010.01.004

Reference yield: 26.7%

{me3SiCH2SC(NH2)2}(+)Br(-) + sodium hydroxide (1310-73-2) → trimethylsilanyl-methanethiol (18165-76-9)

Guidance literature:

In water;

DOI:10.1021/jo50010a020

Reference yield:

Chloromethyltrimethylsilane (2344-80-1) → trimethylsilanyl-methanethiol (18165-76-9)

Guidance literature:

With sodium hydrogensulfide;

DOI:10.1021/ja01638a058

upstream raw materials:

Chloromethyltrimethylsilane

trimethyl(thiocyanatomethyl)silane

chloro-trimethyl-silane

methylthiol

Downstream raw materials:

2-Trimethylsilylmethylthioaethanol

bis<(trimethylsilyl)methyl>sulfide

S-Methyl-S'-trimethylsilylmethyl N-(p-toluenesulfonyl)dithioiminocarbonate

S,S'-Bis(trimethylsilylmethyl) N-(p-toluenesulfonyl)dithioiminocarbonate

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