Disulfide, 2,4-dinitrophenyl pentyl

Base Information

• Chemical Name: Disulfide, 2,4-dinitrophenyl pentyl
• CAS No.: 76919-75-0
• Molecular Formula: C11H14N2O4S2
• Molecular Weight: 302.375

Synonyms:

Chemical Property of Disulfide, 2,4-dinitrophenyl pentyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Disulfide, 2,4-dinitrophenyl pentyl

There total 2 articles about Disulfide, 2,4-dinitrophenyl pentyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

n-pentanethiol (110-66-7) + 2,4-dinitrobenzenesulfenyl chloride (528-76-7) → 2,4-Dinitrophenyl-n-pentyl-disulfid (76919-75-0)

Guidance literature:

In acetic acid; for 3h; Ambient temperature;

DOI:10.1055/s-1980-29252

Reference yield:

→ 2,4-Dinitrophenyl-n-pentyl-disulfid (76919-75-0)

Guidance literature:

B. Behandeln v. 2,4-(NO2)2-C6H3-SCl mit n-Pentylmerkaptan in Aethanol;

Reference yield: 65.0%

2-methylindolizine (768-18-3) + 2,4-Dinitrophenyl-n-pentyl-disulfid (76919-75-0) → bis(2,4-dinitrophenyl) disulphide (2217-55-2) + 2-Methyl-3-pentylsulfanyl-indolizine (76919-79-4)

Guidance literature:

In ethanol; at 50 ℃; for 30h; Yields of byproduct given;

DOI:10.1055/s-1980-29252

upstream raw materials:

n-pentanethiol

2,4-dinitrobenzenesulfenyl chloride

Downstream raw materials:

bis(2,4-dinitrophenyl) disulphide

2-Methyl-3-pentylsulfanyl-indolizine

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