Phosphonothioic diamide, N,N,N',N'-tetramethyl-P-phenyl-

Base Information

Chemical Name:Phosphonothioic diamide, N,N,N',N'-tetramethyl-P-phenyl-
CAS No.:3732-85-2
Molecular Formula:C10H17N2PS
Molecular Weight:228.2941
Hs Code.:
DSSTox Substance ID:DTXSID80190771
Nikkaji Number:J480.251I
Wikidata:Q83063178
Mol file:3732-85-2.mol

Synonyms:Phosphonothioic diamide, N,N,N',N'-tetramethyl-P-phenyl-;N,N,N',N'-Tetramethyl-P-phenylphosphonothioic diamide;3732-85-2;C10H17N2PS;DTXSID80190771;C10-H17-N2-P-S;Bis(dimethylamino)phenylphosphine sulfide

Suppliers and Price of Phosphonothioic diamide, N,N,N',N'-tetramethyl-P-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phosphonothioic diamide, N,N,N',N'-tetramethyl-P-phenyl-

Chemical Property:

Boiling Point:294.3°Cat760mmHg
Flash Point:131.8°C
Density:1.12g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:228.08500672
Heavy Atom Count:14
Complexity:210

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)P(=S)(C1=CC=CC=C1)N(C)C

Technology Process of Phosphonothioic diamide, N,N,N',N'-tetramethyl-P-phenyl-

There total 5 articles about Phosphonothioic diamide, N,N,N',N'-tetramethyl-P-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 124-40-3
dimethyl amine

: 3497-00-5
phenylthiophosphonic acid dichloride

: 3732-85-2
N,N,N',N'-tetramethyl-P-phenylphosphonothioic diamide

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 3.75h; Inert atmosphere;
DOI:10.1002/chir.20702

Reference yield: 71.0%

: 6143-71-1
bis(dimethylamino)phenyl phosphine

: 3732-85-2
N,N,N',N'-tetramethyl-P-phenylphosphonothioic diamide

Guidance literature:: With sulfur; In Petroleum ether;

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 3732-85-2
N,N,N',N'-tetramethyl-P-phenylphosphonothioic diamide

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / petroleum ether / 0.5 h / Ambient temperature

2: 71 percent / sulfur / petroleum ether

With sulfur; In Petroleum ether;