N-[(3-Chlorophenyl)methyl]-4-methoxyaniline

Base Information

Chemical Name:N-[(3-Chlorophenyl)methyl]-4-methoxyaniline
CAS No.:93642-39-8
Molecular Formula:C14H14ClNO
Molecular Weight:247.724
Hs Code.:
DSSTox Substance ID:DTXSID10596161
Wikidata:Q82491340

Synonyms:N-[(3-Chlorophenyl)methyl]-4-methoxyaniline;93642-39-8;SCHEMBL10925112;DTXSID10596161;AKOS000241848

Suppliers and Price of N-[(3-Chlorophenyl)methyl]-4-methoxyaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[(3-Chlorophenyl)methyl]-4-methoxyaniline

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:247.0763918
Heavy Atom Count:17
Complexity:216

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)NCC2=CC(=CC=C2)Cl

Technology Process of N-[(3-Chlorophenyl)methyl]-4-methoxyaniline

There total 4 articles about N-[(3-Chlorophenyl)methyl]-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 104-94-9
4-methoxy-aniline

: 587-04-2
m-Chlorobenzaldehyde

: 93642-39-8
N-(3-chlorobenzyl)-4-methoxybenzenamine

Guidance literature:: With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; iodine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.05.071

Reference yield:

: 18951-47-8
(E)-4-<2-(3-chlorophenyl)ethenyl>phenol

: 2101-87-3
p-methoxy-phenylazide

: 93642-39-8
N-(3-chlorobenzyl)-4-methoxybenzenamine

: 73351-21-0
4-(((4-methoxyphenyl)amino)methyl)phenol

Guidance literature:: (E)-4-<2-(3-chlorophenyl)ethenyl>phenol; p-methoxy-phenylazide; With iron(II) chloride; In acetonitrile; at 100 ℃; for 10h; Sealed tube; Inert atmosphere;

With methanol; sodium tetrahydroborate; at 20 ℃;
DOI:10.1021/acs.orglett.9b03160

Reference yield:

: 2039-85-2,26100-04-9
3-Chlorostyrene

: 93642-39-8
N-(3-chlorobenzyl)-4-methoxybenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate; palladium diacetate / 12 h / 20 °C / Inert atmosphere

2.1: iron(II) chloride / acetonitrile / 10 h / 100 °C / Sealed tube; Inert atmosphere

2.2: 20 °C

With sodium acetate; palladium diacetate; iron(II) chloride; In acetonitrile;
DOI:10.1021/acs.orglett.9b03160