(((Chloromethyl)dimethylsilyl)methyl)trimethylsilane

Base Information

• Chemical Name: (((Chloromethyl)dimethylsilyl)methyl)trimethylsilane
• CAS No.: 18306-73-5
• Molecular Formula: C7H19 Cl Si2
• Molecular Weight: 194.852
• European Community (EC) Number: 242-193-6
• DSSTox Substance ID: DTXSID1066360
• Nikkaji Number: J266.115B
• Wikidata: Q81992959
• Mol file: 18306-73-5.mol

Synonyms:18306-73-5;(((Chloromethyl)dimethylsilyl)methyl)trimethylsilane;chloromethyl-dimethyl-(trimethylsilylmethyl)silane;Silane, [[(chloromethyl)dimethylsilyl]methyl]trimethyl-;[[(chloromethyl)dimethylsilyl]methyl]trimethylsilane;EINECS 242-193-6;(CHLOROMETHYL)DIMETHYL[(TRIMETHYLSILYL)METHYL]SILANE;1-Chloromethyl-1,1,3,3,3-pentamethyldisilylmethylene;Silane, (((chloromethyl)dimethylsilyl)methyl)trimethyl-;1-chloromethyl-1,1,3,3,3-pentamethyl-1,3-disilapropane;(Chloromethyl)dimethyl((trimethylsilyl)methyl)silane;Chloromethyl pentamethyl disilmethylene;C7H19ClSi2;C7-H19-Cl-Si2;1-Chloromethyl-1,1,3,3,3-pentamethyldisilmethylene;SCHEMBL1644229;DTXSID1066360;Chloromethylpentamethyldisilmethylene;MFCD00053232;AKOS006241431;CS-0448908;S04236;1-Chloro-2,2,4,4-tetramethyl-2,4-disilapentane;1-CHLOROMETHYL-1,1,3,3,3-PENTAMETHYL-DISILMETHYLEN

Chemical Property of (((Chloromethyl)dimethylsilyl)methyl)trimethylsilane

Chemical Property:

• Vapor Pressure: 1.15mmHg at 25°C
• Boiling Point: 181.6°Cat760mmHg
• Flash Point: 53.9°C
• PSA: 0.00000
• Density: 0.858g/cm³
• LogP: 3.76850
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 194.0713814
• Heavy Atom Count: 10
• Complexity: 105

Purity/Quality:

98% ^*data from raw suppliers

1-CHLOROMETHYL-1,1,3,3,3-PENTAMETHYLDISILMETHYLENE 95.00% ^*data from reagent suppliers

Safty Information:

• Statements: 11-23/24
• Safety Statements: 9-16-36/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)C[Si](C)(C)CCl

Technology Process of (((Chloromethyl)dimethylsilyl)methyl)trimethylsilane

There total 3 articles about (((Chloromethyl)dimethylsilyl)methyl)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Chloro(chloromethyl)dimethylsilane (1719-57-9) + Chloromethyltrimethylsilane (2344-80-1) → chloromethyl(dimethyl)(trimethylsilylmethyl)silane (18306-73-5)

Guidance literature:

Chloromethyltrimethylsilane; With magnesium; ethylene dibromide; In tetrahydrofuran; for 2h; Schlenk technique; Inert atmosphere; Reflux;

Chloro(chloromethyl)dimethylsilane; In tetrahydrofuran; for 20h; Reflux; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201503901

Reference yield: 85.0%

Chloro(chloromethyl)dimethylsilane (1719-57-9) + trimethylsilylmethyllithium (1822-00-0) → chloromethyl(dimethyl)(trimethylsilylmethyl)silane (18306-73-5)

Guidance literature:

In not given;

Reference yield: 73.0%

Chloro(chloromethyl)dimethylsilane (1719-57-9) + (trimethylsilyl)methylmagnesium chloride (13170-43-9) → chloromethyl(dimethyl)(trimethylsilylmethyl)silane (18306-73-5)

Guidance literature:

In tetrahydrofuran; diethyl ether; for 2h; Heating;

DOI:10.1007/BF02495692

upstream raw materials:

Chloro(chloromethyl)dimethylsilane

(trimethylsilyl)methylmagnesium chloride

trimethylsilylmethyllithium

Chloromethyltrimethylsilane

Downstream raw materials:

2,2,4,4,6,6,8,8,10,10,12,12-dodecamethyl-7-oxa-2,4,6,8,10,12-hexasila-tridecane

1-chloro-2,2,4,4,6,6-hexamethyl-2,4,6-trisila-heptane

octamethyltrisilmethylene

dodecamethylpentasilmethylene