1-Bromo-2-fluoro-4-(methoxymethyl)benzene

Base Information

• Chemical Name: 1-Bromo-2-fluoro-4-(methoxymethyl)benzene
• CAS No.: 162744-47-0
• Molecular Formula: C8H8BrFO
• Molecular Weight: 219.053
• Hs Code.: 2909309090
• Mol file: 162744-47-0.mol

Synonyms:1-Bromo-2-fluoro-4-(methoxymethyl)benzene;Benzene, 1-broMo-2-fluoro-4-(MethoxyMethyl)-

Chemical Property of 1-Bromo-2-fluoro-4-(methoxymethyl)benzene

Chemical Property:

• Boiling Point: 212.6±25.0 °C(Predicted)
• PSA: 9.23000
• Density: 1.470±0.06 g/cm3(Predicted)
• LogP: 2.73460
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-Bromo-2-fluoro-4-(methoxymethyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Bromo-2-fluoro-4-(methoxymethyl)benzene

There total 6 articles about 1-Bromo-2-fluoro-4-(methoxymethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-3-fluorobenzyl alcohol (222978-01-0) + methyl iodide (74-88-4) → 1-bromo-2-fluoro-4-(methoxymethyl)benzene (162744-47-0)

Guidance literature:

4-bromo-3-fluorobenzyl alcohol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.166667h;

methyl iodide; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

Reference yield:

methanol (67-56-1) + 4-Bromo-3-fluorobenzyl methanesulfonate (1240286-88-7) → 1-bromo-2-fluoro-4-(methoxymethyl)benzene (162744-47-0)

Guidance literature:

With 2,6-dimethylpyridine; at 20 ℃; for 88h;

Reference yield:

4-Bromo-3-fluorophenyl + methanesulfonyl chloride (124-63-0) → 1-bromo-2-fluoro-4-(methoxymethyl)benzene (162744-47-0)

Guidance literature:

With sodium methylate; sodium hydrogencarbonate; triethylamine; In methanol; dichloromethane;

upstream raw materials:

methanol

4-Bromo-3-fluorobenzyl methanesulfonate

methyl 4-bromo-3-fluorobenzoate

4-bromo-3-fluorobenzyl alcohol

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