1-(3-Bromopyridin-2-yl)ethanone

Base Information

Chemical Name:1-(3-Bromopyridin-2-yl)ethanone
CAS No.:111043-09-5
Molecular Formula:C7H6BrNO
Molecular Weight:200.03264
Hs Code.:2933399090
European Community (EC) Number:963-226-7
DSSTox Substance ID:DTXSID30572785
Nikkaji Number:J1.395.131D
Wikidata:Q82461269
Mol file:111043-09-5.mol

Synonyms:1-(3-Bromopyridin-2-yl)ethanone;111043-09-5;1-(3-Bromopyridin-2-yl)ethan-1-one;MFCD18257141;2-Acetyl-3-bromopyridine;SCHEMBL5313640;1-(3-bromo-2-pyridyl)ethanone;DTXSID30572785;AMY25992;AKOS015908223;DS-2002;FS-3516;PB39595;SY029920;CS-0018840;EN300-307123

Suppliers and Price of 1-(3-Bromopyridin-2-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-(3-bromopyridin-2-yl)ethanone
250mg
$ 75.00

TRC
1-(3-bromopyridin-2-yl)ethanone
100mg
$ 65.00

TRC
1-(3-bromopyridin-2-yl)ethanone
25mg
$ 45.00

Matrix Scientific
1-(3-Bromopyridin-2-yl)ethanone 95+%
1g
$ 810.00

Matrix Scientific
1-(3-Bromopyridin-2-yl)ethanone 95+%
250mg
$ 324.00

Crysdot
1-(3-Bromopyridin-2-yl)ethanone 95+%
5g
$ 311.00

Crysdot
1-(3-Bromopyridin-2-yl)ethanone 95+%
100g
$ 2814.00

Crysdot
1-(3-Bromopyridin-2-yl)ethanone 95+%
10g
$ 534.00

Crysdot
1-(3-Bromopyridin-2-yl)ethanone 95+%
25g
$ 970.00

Chemenu
2-Acetyl-3-bromopyridine 95%
25g
$ 935.00

Total 34 raw suppliers

Chemical Property of 1-(3-Bromopyridin-2-yl)ethanone

Chemical Property:

Boiling Point:246.0±25.0 °C(Predicted)
PKA:0.40±0.10(Predicted)
PSA：29.96000
Density:1.534±0.06 g/cm3(Predicted)
LogP:2.04670
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:198.96328
Heavy Atom Count:10
Complexity:138

Purity/Quality:

99%, ^*data from raw suppliers

1-(3-bromopyridin-2-yl)ethanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=C(C=CC=N1)Br

Technology Process of 1-(3-Bromopyridin-2-yl)ethanone

There total 4 articles about 1-(3-Bromopyridin-2-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.8%

: 917-64-6
methyl magnesium iodide

: 55758-02-6
3-bromopyridine-2-carbonitrile

: 111043-09-5
1-(3-bromopyridin-2-yl)ethanone

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield: 66.0%

: 75-16-1
methylmagnesium bromide

: 55758-02-6
3-bromopyridine-2-carbonitrile

: 111043-09-5
1-(3-bromopyridin-2-yl)ethanone

Guidance literature:: methylmagnesium bromide; 3-bromopyridine-2-carbonitrile; In tetrahydrofuran; diethyl ether; at -20 - -10 ℃;

With hydrogenchloride; water; In tetrahydrofuran; diethyl ether; at -40 ℃; for 0.0833333h;
DOI:10.1039/c5ob01478f

Reference yield:

: 405174-97-2
3-bromopicolinaldehyde

: 111043-09-5
1-(3-bromopyridin-2-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran / 1 h / -78 - 20 °C

2: Dess-Martin periodane / dichloromethane / 14 h / 0 - 20 °C

With Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane;