2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

Base Information

Chemical Name:2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide
CAS No.:1315478-13-7
Molecular Formula:C13H21N3O2
Molecular Weight:251.329
Hs Code.:
Mol file:1315478-13-7.mol

Synonyms:2-Butyl-1,6-dihydro-N,N,4-trimethyl-6-oxo-5-pyrimidineacetamide;

Suppliers and Price of 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 78 raw suppliers

Chemical Property of 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

Chemical Property:

Boiling Point:385.0±44.0 °C(Predicted)
PKA:9.49±0.50(Predicted)
PSA：66.32000
Density:1.11±0.1 g/cm3(Predicted)
LogP:1.46390

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

There total 6 articles about 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2-(2-n-butyl-4-hydroxy-6-methylpyrimidin-5-yl)-ethanoic acid methyl ester

: 124-40-3
dimethyl amine

: 1315478-13-7
(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Guidance literature:: In methanol; at 115 ℃; for 5h; under 17251.7 Torr; Pressure; Temperature; Autoclave;

Reference yield: 93.0%

: 1315478-16-0
2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid

: 506-59-2
N,N-dimethylammonium chloride

: 1315478-13-7
(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Guidance literature:: 2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid; With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

N,N-dimethylammonium chloride; With chloroformic acid ethyl ester; In dichloromethane; for 12h; Reflux;

With sodium hydroxide; In dichloromethane; water; pH=9;

Reference yield: 87.2%

: 1315478-16-0
2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid

: 124-40-3
dimethyl amine

: 1315478-13-7
(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Guidance literature:: 2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid; With 4-methyl-morpholine; In N,N-dimethyl acetamide; for 0.166667h;

With 1,1'-carbonyldiimidazole; In N,N-dimethyl acetamide; at 20 ℃; for 1h;

dimethyl amine; In tetrahydrofuran; N,N-dimethyl acetamide; at 20 ℃; for 0.5h; Solvent; Concentration;