Dichloro(dichloromethyl)phosphine

Base Information

Chemical Name:Dichloro(dichloromethyl)phosphine
CAS No.:23415-85-2
Molecular Formula:CHCl4P
Molecular Weight:185.805
Hs Code.:2903199000
DSSTox Substance ID:DTXSID40446024
Nikkaji Number:J88.153H
Wikidata:Q82264586
Mol file:23415-85-2.mol

Synonyms:23415-85-2;AGN-PC-0NBPWW;Dichloro(dichloromethyl)phosphine;SCHEMBL10835279;DTXSID40446024

Suppliers and Price of Dichloro(dichloromethyl)phosphine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Dichloro(dichloromethyl)phosphine

Chemical Property:

PSA：13.59000
LogP:3.53710
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:185.854048
Heavy Atom Count:6
Complexity:34.5

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(P(Cl)Cl)(Cl)Cl

Technology Process of Dichloro(dichloromethyl)phosphine

There total 4 articles about Dichloro(dichloromethyl)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 3279-26-3
methyl dichlorophosphite

: 67-66-3,8013-54-5
chloroform

: 23415-85-2
(dichloromethyl)phosphonous dichloride

Guidance literature:: With aluminium trichloride; phosphorus trichloride; Heating; argon atmosphere;

Reference yield:

: 75-09-2
dichloromethane

: 23415-85-2
(dichloromethyl)phosphonous dichloride

: 110-56-5
1,4-dichlorobutane

Guidance literature:: With n-butyllithium; zinc(II) chloride; phosphorus trichloride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) -95 to -80 deg C, 2.5 h; -80 deg C to r.t., 2.) THF, r.t., 30 h;
DOI:10.1021/jo00128a015