Methyl 3-(4-Methoxy-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanoate

Base Information

Chemical Name:Methyl 3-(4-Methoxy-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanoate
CAS No.:1270038-09-9
Molecular Formula:C17H25BO5
Molecular Weight:320.193
Hs Code.:

Synonyms:Methyl 3-(4-Methoxy-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanoate

Suppliers and Price of Methyl 3-(4-Methoxy-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of Methyl 3-(4-Methoxy-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methyl 3-(4-Methoxy-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanoate

There total 3 articles about Methyl 3-(4-Methoxy-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 288310-70-3
3-(3-bromo-4-methoxyphenyl)-propionic acid methyl ester

: 73183-34-3
bis(pinacol)diborane

: 1270038-09-9
methyl 3-[4-methoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propanoate

Guidance literature:: 3-(3-bromo-4-methoxyphenyl)-propionic acid methyl ester; bis(pinacol)diborane; With potassium acetate; In cyclopentylmethyl ether; for 1h; Inert atmosphere;

With dicyclohexylphosphino-2′,4′,6′-triisopropylbiphenyl; palladium diacetate; In cyclopentylmethyl ether; at 80 ℃; for 22h; Inert atmosphere;

Reference yield:

: 53937-17-0
methyl 3-(3-iodo-4-methoxyphenyl)propanoate

: 73183-34-3
bis(pinacol)diborane

: 1270038-09-9
methyl 3-[4-methoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propanoate

Guidance literature:: With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; dimethyl sulfoxide; at 50 - 80 ℃; for 17h; Inert atmosphere;

Reference yield:

: 15823-04-8
methyl 3-(4-methoxyphenyl)propionate

: 1270038-09-9
methyl 3-[4-methoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; silver sulfate / methanol / 1 h / 20 °C

2: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; dimethyl sulfoxide / 17 h / 50 - 80 °C / Inert atmosphere

With iodine; potassium acetate; silver sulfate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; dimethyl sulfoxide;