Vanadinic acid tris(trimethylsilyl) ester

Base Information

Chemical Name:Vanadinic acid tris(trimethylsilyl) ester
CAS No.:5590-56-7
Molecular Formula:C9H27O4Si3V
Molecular Weight:336.52216
Hs Code.:
Mol file:5590-56-7.mol

Synonyms:Vanadinic acid tris(trimethylsilyl) ester

Suppliers and Price of Vanadinic acid tris(trimethylsilyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Vanadinic acid tris(trimethylsilyl) ester

Chemical Property:

PSA：44.76000
LogP:3.78780

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Vanadinic acid tris(trimethylsilyl) ester

There total 4 articles about Vanadinic acid tris(trimethylsilyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: ammonium vanadate(V)

: 5577-67-3
trimethyl(tert-butylamino)silane

: 5590-56-7
Tris-(trimethylsilyl)vanadat

Guidance literature:: With N,N-dimethyl acetamide; under N2; refluxed for ca. 3 h with stirring; addn. of pentane, filtd., the filtrate is evapd., the residue is fractionated, elem. anal.;

Reference yield: 50.0%

: ammonium vanadate(V)

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 5590-56-7
Tris-(trimethylsilyl)vanadat

: 42077-72-5
((trimethylsilyl)imido)tris(trimethylsiloxy)vanadium(V)

Guidance literature:: With N,N-dimethylacetamide; byproducts: NH3; anhydrous and anaerobic conditions; heating (130°C, 4 h), coolingto 25°C; filtn., washing (pentane), solvent removal (vac.), distillation (vac.), recrystallization (pentane, -100°C);
DOI:10.1016/0277-5387(94)00355-I