5-Chloro-2-methylpyridin-3-amine

Base Information

Chemical Name:5-Chloro-2-methylpyridin-3-amine
CAS No.:89639-36-1
Molecular Formula:C6H7ClN2
Molecular Weight:143
Hs Code.:2933399090
DSSTox Substance ID:DTXSID90595854
Wikidata:Q82490949
Mol file:89639-36-1.mol

Synonyms:89639-36-1;5-Chloro-2-methylpyridin-3-amine;3-AMINO-5-CHLORO-2-METHYLPYRIDINE;3-Amino-5-chloropicoline;5-CHLORO-2-METHYL-PYRIDIN-3-YLAMINE;5-chloro-2-methyl-pyridin-3-amine;MFCD12196974;SCHEMBL10144926;DTXSID90595854;AMY29155;CS-M2842;3-Pyridinamine, 5-chloro-2-methyl-;AKOS015910063;PB22604;AS-34110;SY026555;DB-348072;EN300-171254;A843259

Suppliers and Price of 5-Chloro-2-methylpyridin-3-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Amino-5-chloro-2-methylpyridine
100mg
$ 65.00

SynQuest Laboratories
5-Chloro-2-methylpyridin-3-amine
1 g
$ 310.00

SynQuest Laboratories
5-Chloro-2-methylpyridin-3-amine
5 g
$ 980.00

J&W Pharmlab
5-Chloro-2-methyl-pyridin-3-ylamine 97%
5g
$ 950.00

J&W Pharmlab
5-Chloro-2-methyl-pyridin-3-ylamine 97%
1g
$ 298.00

Crysdot
5-Chloro-2-methylpyridin-3-amine 95+%
25g
$ 1140.00

Crysdot
5-Chloro-2-methylpyridin-3-amine 95+%
10g
$ 633.00

Crysdot
5-Chloro-2-methylpyridin-3-amine 95+%
5g
$ 422.00

Crysdot
5-Chloro-2-methylpyridin-3-amine 95+%
1000g
$ 11400.00

Crysdot
5-Chloro-2-methylpyridin-3-amine 95+%
500g
$ 7505.00

Total 30 raw suppliers

Chemical Property of 5-Chloro-2-methylpyridin-3-amine

Chemical Property:

PSA：38.91000
LogP:2.20680
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:142.0297759
Heavy Atom Count:9
Complexity:97.1

Purity/Quality:

99%, ^*data from raw suppliers

3-Amino-5-chloro-2-methylpyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=N1)Cl)N

Technology Process of 5-Chloro-2-methylpyridin-3-amine

There total 3 articles about 5-Chloro-2-methylpyridin-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1211533-93-5
2-methyl-3-nitro-5-chloropyridine

: 89639-36-1
5-chloro-2-methylpyridin-3-amine

Guidance literature:: With tin(II) chloride dihdyrate; In ethyl acetate; at 85 ℃; for 3h; Inert atmosphere;

Reference yield:

: 78607-32-6
3-amino-2,5-dichloropyridine

: 13061-96-6
dihydroxy-methyl-borane

: 89639-36-1
5-chloro-2-methylpyridin-3-amine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; In 1,2-dimethoxyethane; water; at 120 ℃; for 12h; Inert atmosphere;

Reference yield:

: 21427-62-3
2,5-dichloro-3-nitropyridine

: 89639-36-1
5-chloro-2-methylpyridin-3-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 3.83 h / 20 °C / Inert atmosphere

1.2: 12.5 h / Reflux

1.3: pH 9

2.1: tin(II) chloride dihdyrate / ethyl acetate / 3 h / 85 °C / Inert atmosphere

With tin(II) chloride dihdyrate; sodium hydride; In tetrahydrofuran; ethyl acetate; mineral oil;