1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine

Base Information

Chemical Name:1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine
CAS No.:1255909-21-7
Molecular Formula:C₁₅H₂₇NO₄SSi
Molecular Weight:345.535
Hs Code.:
Mol file:1255909-21-7.mol

Synonyms:1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine

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Chemical Property of 1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine

Chemical Property:

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Technology Process of 1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine

There total 1 articles about 1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-71-0
dimethylsulfone

: 1131-52-8
3-ethoxy-4-methoxybenzaldehyde

: 4039-32-1
lithium hexamethyldisilazane

: 1255909-21-7
1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine

Guidance literature:: dimethylsulfone; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

3-ethoxy-4-methoxybenzaldehyde; lithium hexamethyldisilazane; With boron trifluoride; In tetrahydrofuran; diethyl ether; hexane; at 20 ℃; Cooling with salt-ice; Inert atmosphere;

Reference yield:

: 1255909-21-7
1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine

: 608141-42-0
(S)-2-[1 (3-ethoxy-4-methoxyphenyl)]-1-methanesulfonyl-2-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / diethyl ether / 0.5 h / 20 °C

1.2: pH 12 / Cooling with ice

2.1: methanol / 8 h / 20 °C / Inert atmosphere; Reflux

3.1: sodium hydroxide / dichloromethane; water / pH 11 / Cooling with ice

With hydrogenchloride; water; sodium hydroxide; In methanol; diethyl ether; dichloromethane; water;

Reference yield:

: 1255909-21-7
1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine

: 253168-94-4
2-(3-ethoxy-4-methoxyphenyl)-1-(methylsulfonyl)eth-2-ylamine

Guidance literature:: 1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)-N-(trimethylsilyl)ethylamine; With hydrogenchloride; water; In diethyl ether; at 20 ℃; for 0.5h;

With sodium hydroxide; In water; pH=12; Cooling with ice;