(2-chloro-4-morpholin-4-yl-thieno[3,2-d]pyrimidin-6-ylmethyl)-methyl-amine

Base Information

• Chemical Name: (2-chloro-4-morpholin-4-yl-thieno[3,2-d]pyrimidin-6-ylmethyl)-methyl-amine
• CAS No.: 955979-15-4
• Molecular Formula: C12H15ClN4OS
• Molecular Weight: 298.796
• Mol file: 955979-15-4.mol

Synonyms:(2-chloro-4-morpholin-4-yl-thieno[3,2-d]pyrimidin-6-ylmethyl)-methyl-amine;Thieno[3,2-d]pyrimidine-6-methanamine, 2-chloro-N-methyl-4-(4-morpholinyl)-;1-(2-chloro-4-morpholinothieno[3,2-d]pyrimidin-6-yl)-N-methylmethanamine

Chemical Property of (2-chloro-4-morpholin-4-yl-thieno[3,2-d]pyrimidin-6-ylmethyl)-methyl-amine

Chemical Property:

• PSA: 78.52000
• Density: 1.380±0.06 g/cm3 (20 °C, 760 mmHg)
• LogP: 2.35660
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

98% ^*data from raw suppliers

1-(2-Chloro-4-morpholinothieno[3,2-d]pyrimidin-6-yl)-N-methylmethanamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-chloro-4-morpholin-4-yl-thieno[3,2-d]pyrimidin-6-ylmethyl)-methyl-amine

There total 14 articles about (2-chloro-4-morpholin-4-yl-thieno[3,2-d]pyrimidin-6-ylmethyl)-methyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.9%

2-chloro-4-morpholinothieno[3,2-d]pyrimidine-6-carbaldehyde (885618-31-5) + methylamine (74-89-5) → 1-(2-chloro-4-morpholinothieno[3,2-d]pyrimidin-6-yl)-N-methylmethanamine (955979-15-4)

Guidance literature:

2-chloro-4-morpholinothieno[3,2-d]pyrimidine-6-carbaldehyde; methylamine; In methanol; at 20 - 30 ℃; Large scale;

With sodium tetrahydroborate; at 20 - 30 ℃; Large scale;

Reference yield: 85.0%

2-chloro-4-morpholinothieno[3,2-d]pyrimidine-6-carbaldehyde (885618-31-5) → 1-(2-chloro-4-morpholinothieno[3,2-d]pyrimidin-6-yl)-N-methylmethanamine (955979-15-4)

Guidance literature:

2-chloro-4-morpholinothieno[3,2-d]pyrimidine-6-carbaldehyde; In methanol; methylamine; at 20 ℃; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;

Reference yield: 85.0%

C12H13ClN2OS + methylamine (74-89-5) → 1-(2-chloro-4-morpholinothieno[3,2-d]pyrimidin-6-yl)-N-methylmethanamine (955979-15-4)

Guidance literature:

C₁₂H₁₃ClN₂OS; methylamine; In methanol; at 20 ℃; Inert atmosphere;

With sodium tetrahydroborate; at 20 ℃; Inert atmosphere;

upstream raw materials:

2-chloro-4-morpholinothieno[3,2-d]pyrimidine-6-carbaldehyde

2,4-dichlorothieno[3,2-d]pyrimidine

2-chloro-4-morpholinothieno[3,2-d]pyrimidine

2-chloro-4-morpholinylthiophene[3,2-d]pyrimidine-6-methanol

Downstream raw materials:

N-((2-chloro-4-morpholinothieno[3,2-d]pyrimidin-6-yl)methyl)-N-methylbenzamide

N-((2-(3-hydroxyphenyl)-4-morpholinothieno[3,2-d]pyrimidin-6-yl)methyl)-N-methylacrylamide

tert-butyl (2-(3-hydroxyphenyl)-4-morpholinothieno[3,2-d]pyrimidin-6-yl)methyl(methyl)carbamate

3-(6-((methylamino)methyl)-4-morpholinothieno[3,2-d]pyrimidin-2-yl)phenol

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