2-(Diphenylphosphanyl)-n,n-dimethylethanamine

Base Information

• Chemical Name: 2-(Diphenylphosphanyl)-n,n-dimethylethanamine
• CAS No.: 29679-67-2
• Molecular Formula: C16H20 N P
• Molecular Weight: 257.315
• NSC Number: 118386
• DSSTox Substance ID: DTXSID10297823
• Nikkaji Number: J1.091.647J
• Wikidata: Q82039285
• Mol file: 29679-67-2.mol

Synonyms:2-(diphenylphosphanyl)-n,n-dimethylethanamine;29679-67-2;NSC118386;2-diphenylphosphanyl-N,N-dimethylethanamine;SCHEMBL3164447;DTXSID10297823;NSC-118386;1-dimethylamino-2-diphenylphosphinoethane;2-diphenylphosphanyl-N,N-dimethyl-ethanamine;CS-0310195;2-(Diphenylphosphanyl)-N,N-dimethylethan-1-amine

Chemical Property of 2-(Diphenylphosphanyl)-n,n-dimethylethanamine

Chemical Property:

• Vapor Pressure: 6.77E-05mmHg at 25°C
• Boiling Point: 344°Cat760mmHg
• Flash Point: 161.9°C
• Density: g/cm³
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 257.133336640
• Heavy Atom Count: 18
• Complexity: 199

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)CCP(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of 2-(Diphenylphosphanyl)-n,n-dimethylethanamine

There total 4 articles about 2-(Diphenylphosphanyl)-n,n-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

potassium diphenylphosphine (15475-27-1,4346-39-8) → N,N-dimethyl-2-diphenylphosphinoethylamine (29679-67-2)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1055/s-0028-1088060

Reference yield: 76.0%

(2-chloroethyl)dimethylamine hydrochloride (4584-46-7) + diphenylphosphane (829-85-6) → N,N-dimethyl-2-diphenylphosphinoethylamine (29679-67-2)

Guidance literature:

diphenylphosphane; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.25h;

(2-chloroethyl)dimethylamine hydrochloride; In tetrahydrofuran; at 75 ℃; for 16h;

DOI:10.1246/bcsj.81.127

Reference yield:

2-(dimethylamino)ethyl chloride (107-99-3) + lithium diphenylphosphide (65567-06-8,4541-02-0) → N,N-dimethyl-2-diphenylphosphinoethylamine (29679-67-2)

Guidance literature:

In tetrahydrofuran; benzene; Heating;

DOI:10.1021/ja00528a037

upstream raw materials:

2-(dimethylamino)ethyl chloride

lithium diphenylphosphide

(2-chloroethyl)dimethylamine hydrochloride

diphenylphosphane

Downstream raw materials:

(β-N,N-dimethylaminoethyl)benzyldiphenylphosphonium bromide

P-(N,N-dimethylaminoethyl)-P,P-diphenylphosphine oxide

[PtCl(C₆H₅)((C₆H₅)2PCH₂CH₂N(CH₃)2)]

chlorocarbonyl(2-(diphenylphosphino)-N,N-dimethylethylamine)iridium(I)

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