(2-Chloro-3-pyridinyl)-N-methylmethanamine

Base Information

• Chemical Name: (2-Chloro-3-pyridinyl)-N-methylmethanamine
• CAS No.: 120739-88-0
• Molecular Formula: C7H9ClN2
• Molecular Weight: 156.615
• Hs Code.: 2933399090
• Mol file: 120739-88-0.mol

Synonyms:(2-Chloro-3-pyridinyl)-N-methylmethanamine;(2-chloropyridin-3-yl)-N-methylmethanamine;2-Chloro-3-[(methylamino)methyl]pyridine

Chemical Property of (2-Chloro-3-pyridinyl)-N-methylmethanamine

Chemical Property:

• PSA: 24.92000
• LogP: 1.84530
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

98%min ^*data from raw suppliers

1-(2-Chloropyridin-3-yl)-n-methylmethanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-Chloro-3-pyridinyl)-N-methylmethanamine

There total 3 articles about (2-Chloro-3-pyridinyl)-N-methylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-chloro-3-carbaldehydepyridine (36404-88-3) + methylamine (74-89-5) → (2-chloro-pyridin-3-ylmethyl)-methyl-amine (120739-88-0)

Guidance literature:

2-chloro-3-carbaldehydepyridine; methylamine; In methanol; at 20 ℃; for 24h;

With sodium tetrahydroborate; at 0 ℃; for 2h;

Reference yield:

C7H7ClN2 → (2-chloro-pyridin-3-ylmethyl)-methyl-amine (120739-88-0)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃;

DOI:10.1016/j.tetlet.2010.05.121

Reference yield:

2-chloropyridine (109-09-1) → (2-chloro-pyridin-3-ylmethyl)-methyl-amine (120739-88-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 41 percent / LDA / tetrahydrofuran / -70 °C

2: NABH₄ / methanol

With sodium tetrahydroborate; lithium diisopropyl amide; In tetrahydrofuran; methanol;

DOI:10.3987/COM-05-S(T)64

upstream raw materials:

2-chloro-3-carbaldehydepyridine

methylamine

2-chloropyridine

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