1,1'-(2,6-Pyridinediyl)bis(ethanone 2-hydroxybenzoylhydrazone)

Base Information

Chemical Name:1,1'-(2,6-Pyridinediyl)bis(ethanone 2-hydroxybenzoylhydrazone)
CAS No.:76115-25-8
Molecular Formula:C23H21N5O4
Molecular Weight:0
Hs Code.:
Mol file:76115-25-8.mol

Synonyms:1,1'-(2,6-Pyridinediyl)bis(ethanone 2-hydroxybenzoylhydrazone);2,6-Bis(1-salicyloylhydrazonoethyl)pyridine;2,6-Bis[1-[2-(o-hydroxybenzoyl)hydrazono]ethyl]pyridine;2,6-Diacetylpyridine bis(2-hydroxybenzoylhydrazone);2,6-Diacetylpyridinebis(salicyloylhydrazone);N',N'''-[2,6-Pyridinediylbis(ethan-1-yl-1-ylidene)]bis(2-hydroxybenzenecarbohydrazide)

Suppliers and Price of 1,1'-(2,6-Pyridinediyl)bis(ethanone 2-hydroxybenzoylhydrazone)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,1'-(2,6-Pyridinediyl)bis(ethanone 2-hydroxybenzoylhydrazone)

Chemical Property:

Melting Point:234 °C
PSA：143.25000
LogP:3.95040

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1'-(2,6-Pyridinediyl)bis(ethanone 2-hydroxybenzoylhydrazone)

There total 1 articles about 1,1'-(2,6-Pyridinediyl)bis(ethanone 2-hydroxybenzoylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1129-30-2
2,6-Diacetylpyridine

: 936-02-7
2-Hydroxybenzoylhydrazine

: 76115-25-8
2,6-diacetylpyridine bis(salicyloylhydrazone)

Guidance literature:: In ethanol; benzene; for 1h; Heating;
DOI:10.1039/DT9800001970

Reference yield: 95.0%

: 7439-92-1
lead

: 7732-18-5
water

: 76115-25-8
2,6-diacetylpyridine bis(salicyloylhydrazone)

: 75-05-8,26809-02-9
acetonitrile

: Pb(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(H₂O)2

: [Et₄N][Pb(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(CN)]

Guidance literature:: With tetraethylammonium perchlorate; In acetonitrile; Electrolysis; suspn. of ligand in MeCN contg. Et4NClO4 electrolysed for 24 h, Pb plateas anode, 10 mA current; filtered; solid washed with Et2O; dried under vac. (Pb-2H2O complex); crystd. by concn. of mother liquor (Pb-CN complex); elem. anal.;
DOI:10.1039/b610010d

Reference yield: 93.0%

: 7440-31-5
tin

: 7732-18-5
water

: 76115-25-8
2,6-diacetylpyridine bis(salicyloylhydrazone)

: Sn(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(H₂O)3

: [Sn(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(H₂O)2]*4H₂O

Guidance literature:: With tetraethylammonium perchlorate; In acetonitrile; Electrolysis; suspn. of ligand in MeCN contg. Et4NClO4 electrolysed for 24 h, Sn plateas anode, 10 mA current; filtered; solid washed with Et2O; dried under vac.; elem. anal.;
DOI:10.1039/b610010d