methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

Base Information

Chemical Name:methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate
CAS No.:1338243-88-1
Molecular Formula:C₁₆H₂₁NO₄
Molecular Weight:291.347
Hs Code.:
Mol file:1338243-88-1.mol

Synonyms:methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

Suppliers and Price of methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

TRC
methyl4-(1-{[(tert-butoxy)carbonyl]amino}cyclopropyl)benzoate
100mg
$ 285.00

Total 4 raw suppliers

Chemical Property of methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

methyl4-(1-{[(tert-butoxy)carbonyl]amino}cyclopropyl)benzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

There total 7 articles about methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 67-56-1
methanol

: 360773-84-8
tert-butyl [1-(4-bromophenyl)-cyclopropyl]-carbamate

: 201230-82-2
carbon monoxide

: 1338243-88-1
methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; at 130 ℃;

Reference yield:

: 1006037-03-1
4-(1-aminocyclopropyl)-benzoic acid methyl ester

: 24424-99-5
di-tert-butyl dicarbonate

: 1338243-88-1
methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

Guidance literature:: In acetonitrile; at 20 ℃; for 6h;

Reference yield:

: 345965-52-8
1-(4-bromophenyl)cyclopropanecarboxylic acid

: 1338243-88-1
methyl 4-(1-((tert-butoxycarbonyl)amino)cyclopropyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / toluene / 5 h / Molecular sieve; Reflux

2: triethylamine; 1,3-bis-(diphenylphosphino)propane / palladium diacetate / N,N-dimethyl-formamide; methanol / 48 h / 80 °C / 30003 Torr

With diphenyl phosphoryl azide; 1,3-bis-(diphenylphosphino)propane; triethylamine; N-ethyl-N,N-diisopropylamine; palladium diacetate; In methanol; N,N-dimethyl-formamide; toluene;