methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate

Base Information

Chemical Name:methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate
CAS No.:1462949-88-7
Molecular Formula:C₁₅H₁₂N₂O₂S₂
Molecular Weight:316.404
Hs Code.:
Mol file:1462949-88-7.mol

Synonyms:methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate

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Chemical Property of methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate

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Technology Process of methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate

There total 4 articles about methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1462949-85-4
methyl 2-(methylsulfanyl)-7-{[(trifluoromethyl)sulfonyl]oxy}thieno[3,2-d]pyrimidine-6-carboxylate

: 98-80-6
phenylboronic acid

: 1462949-88-7
methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert-butylimino-tri(pyrrolidino)phosphorane; In 1,4-dioxane; for 20h; Inert atmosphere; Reflux;

Reference yield:

: 61727-33-1
5-chloro-2-(methylthio)pyrimidine-4-carboxylic acid

: 1462949-88-7
methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: chloro-trimethyl-silane / dichloromethane / 20 h / 20 °C

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3.25 h / 20 - 60 °C

3: pyridine / 48 h / 20 °C

4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert-butylimino-tri(pyrrolidino)phosphorane / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; chloro-trimethyl-silane; sodium hydride; tert-butylimino-tri(pyrrolidino)phosphorane; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 79686-03-6
methyl 5-chloro-2-(methylsulfanyl)pyrimidine-4-carboxylate

: 1462949-88-7
methyl 2-(methylsulfanyl)-7-phenylthieno[3,2-d]pyrimidine-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3.25 h / 20 - 60 °C

2: pyridine / 48 h / 20 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert-butylimino-tri(pyrrolidino)phosphorane / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydride; tert-butylimino-tri(pyrrolidino)phosphorane; In 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;