2-(2-methylpiperidin-1-yl)ethanol(SALTDATA: FREE)

Base Information

• Chemical Name: 2-(2-methylpiperidin-1-yl)ethanol(SALTDATA: FREE)
• CAS No.: 17719-74-3
• Molecular Formula: C8H17NO
• Molecular Weight: 143.229
• Hs Code.: 2933399090
• DSSTox Substance ID: DTXSID10504347
• Mol file: 17719-74-3.mol

Synonyms:2-(2-methylpiperidin-1-yl)ethanol(SALTDATA: FREE)

Chemical Property of 2-(2-methylpiperidin-1-yl)ethanol(SALTDATA: FREE)

Chemical Property:

• PSA: 23.47000
• LogP: 0.79100
• XLogP3: 0.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 143.131014166
• Heavy Atom Count: 10
• Complexity: 95.3

Purity/Quality:

97% ^*data from raw suppliers

2-(2-methylpiperidin-1-yl)ethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CCCCN1CCO

Technology Process of 2-(2-methylpiperidin-1-yl)ethanol(SALTDATA: FREE)

There total 4 articles about 2-(2-methylpiperidin-1-yl)ethanol(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-Methylpiperidin (109-05-7,3000-79-1) + 2-bromoethanol (540-51-2) → 1-(2-hydroxyethyl)-2-methylpiperidine (17719-74-3)

Guidance literature:

at 80 ℃; for 72h;

Reference yield:

oxirane (75-21-8,99932-75-9) + 2-Methylpiperidin (109-05-7,3000-79-1) → 1-(2-hydroxyethyl)-2-methylpiperidine (17719-74-3)

Guidance literature:

With methanol;

DOI:10.1021/ja01178a028

Reference yield:

6-methyl-2,3,4,5-tetrahydro-pyridine (1462-92-6) + 1-bromo-2-[(trimethylsilyl)oxy]ethane (34714-03-9) → 1-(2-hydroxyethyl)-2-methylpiperidine (17719-74-3) + 2-(3-hydroxypropyl)piperidine (24448-89-3,33078-63-6)

Guidance literature:

With sodium tetrahydroborate; lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given;

upstream raw materials:

oxirane

2-Methylpiperidin

2-bromoethanol

6-methyl-2,3,4,5-tetrahydro-pyridine

Downstream raw materials:

(+/-)-N-(2-Chloroethyl)-2-methylpiperidine

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