Benzenepropanoic acid, 4-bromo-β-methyl-, methyl ester

Base Information

Chemical Name:Benzenepropanoic acid, 4-bromo-β-methyl-, methyl ester
CAS No.:1021735-42-1
Molecular Formula:C11H13BrO2
Molecular Weight:257.127
Hs Code.:
Mol file:1021735-42-1.mol

Synonyms:Benzenepropanoic acid, 4-bromo-β-methyl-, methyl ester;methyl(S)-3-(4-bromophenyl)butanoate

Suppliers and Price of Benzenepropanoic acid, 4-bromo-β-methyl-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Methyl3-(4-Bromophenyl)butanoate
10mg
$ 45.00

AK Scientific
Methyl3-(4-bromophenyl)butanoate
250mg
$ 361.00

AK Scientific
Methyl3-(4-bromophenyl)butanoate
100mg
$ 283.00

Total 1 raw suppliers

Chemical Property of Benzenepropanoic acid, 4-bromo-β-methyl-, methyl ester

Chemical Property:

PSA：26.30000
LogP:3.11570

Purity/Quality:: Methyl3-(4-Bromophenyl)butanoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanoic acid, 4-bromo-β-methyl-, methyl ester

There total 3 articles about Benzenepropanoic acid, 4-bromo-β-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 2077-19-2
2-(4-bromophenyl)propan-2-ol

: 1021735-42-1
methyl 3-(4-bromophenyl)butanoate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; α,α′-bis(2-pyridyl(tert-butyl)phosphino)-o-xylene; toluene-4-sulfonic acid; at 100 ℃; for 20h; under 15001.5 Torr; Autoclave; Inert atmosphere;
DOI:10.1002/anie.201701950

Reference yield: 47.0%

: 3650-78-0,84878-00-2,71205-17-9
methyl (E)-4-bromocinnamate

: 676-58-4
methylmagnesium chloride

: 1021735-42-1
methyl 3-(4-bromophenyl)butanoate

Guidance literature:: With chloro-trimethyl-silane; copper(I) thiophenolate; In tetrahydrofuran; diethyl ether; at -78 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.1021/jm301470a

Reference yield:

: 3650-78-0,84878-00-2,71205-17-9
methyl (E)-4-bromocinnamate

: 917-54-4
methyllithium

: 1021735-42-1
methyl 3-(4-bromophenyl)butanoate

Guidance literature:: methyllithium; With copper(l) iodide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.333333h;

methyl (E)-4-bromocinnamate; In tetrahydrofuran; diethyl ether; at 0 ℃; for 2.5h;

With ammonium chloride; In tetrahydrofuran; diethyl ether;