3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)oxazolidin-2-one

Base Information

Chemical Name:3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)oxazolidin-2-one
CAS No.:1346253-82-4
Molecular Formula:C₁₅H₂₀BNO₄
Molecular Weight:289.139
Hs Code.:
Mol file:1346253-82-4.mol

Synonyms:3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)oxazolidin-2-one

Suppliers and Price of 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)oxazolidin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)oxazolidin-2-one

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)oxazolidin-2-one

There total 2 articles about 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 124-38-9,18923-20-1
carbon dioxide

: 106-93-4
ethylene dibromide

: 214360-73-3
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

: 1346253-82-4
3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3-oxazolidin-2-one

Guidance literature:: With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; caesium carbonate; In acetonitrile; at 60 ℃; for 20h; under 750.075 Torr; Glovebox; Inert atmosphere;
DOI:10.1002/chem.201602338

Reference yield:

: 22036-26-6
3-(4-aminophenyl)-1,3-oxazolidin-2-one

: 73183-34-3
bis(pinacol)diborane

: 1346253-82-4
3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3-oxazolidin-2-one

Guidance literature:: With tert.-butylnitrite; dibenzoyl peroxide; In acetonitrile; at 20 ℃;

Reference yield: 24.0%

: 1384958-64-8
(1E,4E)-ethyl 2-amino-7-bromo-3H-benzo[b]azepine-4-carboxylate

: 1346253-82-4
3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3-oxazolidin-2-one

: 1386859-80-8
ethyl 2-amino-7-[4-(2-oxo-1,3-oxazolidin-3-yl)phenyl]-3H-1-benzazepine-4-carboxylate

Guidance literature:: (1E,4E)-ethyl 2-amino-7-bromo-3H-benzo[b]azepine-4-carboxylate; 3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3-oxazolidin-2-one; With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; dichloromethane; water; toluene; at 80 ℃; Inert atmosphere;

With acetic acid; In dichloromethane;

With sodium hydrogencarbonate; In dichloromethane; for 1h;