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9-Cl-o-HCB10H9CH

Base Information
  • Chemical Name:9-Cl-o-HCB10H9CH
  • CAS No.:19513-12-3
  • Molecular Formula:C2H11B10Cl
  • Molecular Weight:178.672
  • Hs Code.:
9-Cl-o-HCB<sub>10</sub>H<sub>9</sub>CH

Synonyms:9-Cl-o-HCB10H9CH

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Chemical Property of 9-Cl-o-HCB10H9CH
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Technology Process of 9-Cl-o-HCB10H9CH

There total 2 articles about 9-Cl-o-HCB10H9CH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With potassium permanganate; sodium; In ammonia; redn. with 2 equival. Na in liq. NH3, oxidn. with KMnO4;; 5% m-carborane, 10% o-carborane, 23% 9-Cl-o-carborane, 15% 3-amino-o-carborane;;
Guidance literature:
In tetrachloromethane; refluxing soln. of I2, o-carborane and AlCl3 in CCl4 under N2 for 3 h;; pouring into distd. water; separation of organic layer; drying over MgSO4; filtration; concentrating; product mixt. obtained; gas chromatography; separation by preparative gas chromatography; elem. anal.; mass spectroscopy; NMR spectroscopy;;
Guidance literature:
With potassium permanganate; sodium; In ammonia; redn. with 2 equival. Na in liq. NH3, oxidn. with KMnO4;; 27% o-carborane, 20% 3-amino-o-carborane;;
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