2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide

Base Information Edit

Chemical Name:2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide
CAS No.:99802-96-7
Molecular Formula:C₁₂H₁₃N₂O*I
Molecular Weight:328.153
Hs Code.:
Mol file:99802-96-7.mol

Synonyms:2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide

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Chemical Property of 2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide Edit

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Technology Process of 2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide

There total 5 articles about 2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 30148-17-5
(1-methyl-1H-imidazol-2-yl)(phenyl)methanone

: 74-88-4
methyl iodide

: 99802-96-7
2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide

Guidance literature:: In 1,4-dioxane; at 70 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.8b02567

Reference yield:

: 616-47-7
1-methyl-1H-imidazole

: 98-88-4
benzoyl chloride

: 74-88-4
methyl iodide

: 99802-96-7
2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide

Guidance literature:: 1-methyl-1H-imidazole; benzoyl chloride; With dmap; triethylamine; In chloroform; at 0 - 20 ℃; for 12h; Inert atmosphere;

methyl iodide; In 1,4-dioxane; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tetlet.2020.152532

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 99802-96-7
2-benzoyl-1,3-dimethyl-1H-imidazol-3-ium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1.6 M butyllithium / 1.) THF, hexane, -78 deg C, 15 min; 2.) THF, allowed to r.t. during 30 min

2: 66.7 percent / ethyl acetate / 5 h / 95 - 100 °C

With n-butyllithium; In ethyl acetate;