tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate

Base Information

Chemical Name:tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate
CAS No.:1391739-80-2
Molecular Formula:C₂₄H₃₅N₃O₄
Molecular Weight:429.56
Hs Code.:

Synonyms:tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate

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Chemical Property of tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate

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Technology Process of tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate

There total 8 articles about tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 879275-33-9
(R)-1-piperidin-3-ylmethyl-carbamic acid tert-butyl ester

: 87341-45-5
(2S)-N-(4-methylbenzyl) pyroglutamic acid

: 1391739-80-2
tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 3.16667h; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 879275-33-9
(R)-1-piperidin-3-ylmethyl-carbamic acid tert-butyl ester

: (S)-1-(4-Methyl-benzyl)-5-oxo-pyrrolidine-2-carbonyl chloride

: 1391739-80-2
tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate

Guidance literature:: (R)-1-piperidin-3-ylmethyl-carbamic acid tert-butyl ester; With triethylamine; In dichloromethane; at 0 ℃;

(S)-1-(4-Methyl-benzyl)-5-oxo-pyrrolidine-2-carbonyl chloride; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

: 1016167-99-9
(S)-1-piperidin-3-ylmethylcarbamic acid tert-butyl ester

: (S)-1-(4-Methyl-benzyl)-5-oxo-pyrrolidine-2-carbonyl chloride

: 1391739-80-2
tert-butyl ((S)-1-((S)-1-(4-methylbenzyl)-5-oxopyrrolidine-2-carbonyl)piperidin-3-yl)methylcarbamate

Guidance literature:: (S)-1-piperidin-3-ylmethylcarbamic acid tert-butyl ester; With triethylamine; In dichloromethane; at 0 ℃;

(S)-1-(4-Methyl-benzyl)-5-oxo-pyrrolidine-2-carbonyl chloride; In dichloromethane; at 0 - 20 ℃; for 3h;