3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

Base Information

Chemical Name:3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester
CAS No.:135388-94-2
Molecular Formula:C₂₄H₂₁NO₉
Molecular Weight:467.432
Hs Code.:

Synonyms:3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

Suppliers and Price of 3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

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Chemical Property of 3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

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Technology Process of 3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

There total 1 articles about 3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14719-83-6
methyl 3-nitro-4-chlorobenzoate

: 135388-93-1
5-Benzyloxy-3-hydroxy-4-methoxybenzoesaeuremethylester

: 135388-94-2
3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 20 deg C, 15 min 2.) 125 deg C, 45 min;
DOI:10.1055/s-1991-26496

Reference yield: 70.0%

: 64-17-5
ethanol

: 135388-94-2
3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

: 135388-95-3
2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

Guidance literature:: With hydrogenchloride; tin(ll) chloride; at 20 ℃; for 12h;
DOI:10.1055/s-1991-26496

Reference yield:

: 135388-94-2
3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

: 104290-38-2
perrottetin G

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / SnCl₂, HCl / 12 h / 20 °C

2: 1.) NaNO₂, AcOH, 15 percent HCl 2.) 30 percent H₃PO₂ / 1.) H₂O, 0 deg C, 20 min 2.) 0 deg C, 12 h

3: 1.) LiAlH₄ 2.) H₂SO₄ / 1.) THF, 20 deg C, 15 h 2.) H₂O, 0 deg C

4: 1.) Br₃B / 1.) CH₂Cl₂, 20 deg C, 3 h 2.) MeCN, reflux, 1 h

5: 1.) NaOMe / 1.) MeOH, 20 deg C, 30 min 2.) reflux, 2 h

6: 94 percent / H₂ / 5 percent Pd-C / methanol / 12 h / 20 °C / 3750.3 Torr

With hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; hydrogen; sodium methylate; hypophosphorous acid; boron tribromide; acetic acid; tin(ll) chloride; sodium nitrite; palladium on activated charcoal; In methanol;
DOI:10.1055/s-1991-26496